2-amino-6-benzyloxy-9-<2'-(2,2-dimethyl-1,3-dioxan-5-yl)-ethyl>-9H-purine

Base Information

Chemical Name:2-amino-6-benzyloxy-9-<2'-(2,2-dimethyl-1,3-dioxan-5-yl)-ethyl>-9H-purine
CAS No.:127205-15-6
Molecular Formula:C₂₀H₂₅N₅O₃
Molecular Weight:383.45
Hs Code.:

Synonyms:2-amino-6-benzyloxy-9-<2'-(2,2-dimethyl-1,3-dioxan-5-yl)-ethyl>-9H-purine

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Chemical Property of 2-amino-6-benzyloxy-9-<2'-(2,2-dimethyl-1,3-dioxan-5-yl)-ethyl>-9H-purine

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Technology Process of 2-amino-6-benzyloxy-9-<2'-(2,2-dimethyl-1,3-dioxan-5-yl)-ethyl>-9H-purine

There total 6 articles about 2-amino-6-benzyloxy-9-<2'-(2,2-dimethyl-1,3-dioxan-5-yl)-ethyl>-9H-purine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6482-32-2
2-(hydroxymethyl)butane-1,4-diol

: 127205-15-6
2-amino-6-benzyloxy-9-<2'-(2,2-dimethyl-1,3-dioxan-5-yl)-ethyl>-9H-purine

Guidance literature:: Multi-step reaction with 4 steps

1: 41 percent / p-TsOH*H₂O / tetrahydrofuran / 0.5 h / Ambient temperature

2: 87 percent / CBr₄, PPh₃ / dimethylformamide / 0.5 h / 0 °C

3: 64 percent / K₂CO₃ / dimethylformamide / 5 h / Ambient temperature

With carbon tetrabromide; potassium carbonate; toluene-4-sulfonic acid; triphenylphosphine; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/jm00392a020

Reference yield:

: 7459-46-3
triethyl 1,1,2-ethanetricarboxylate

: 127205-15-6
2-amino-6-benzyloxy-9-<2'-(2,2-dimethyl-1,3-dioxan-5-yl)-ethyl>-9H-purine

Guidance literature:: Multi-step reaction with 5 steps

1: 100 percent / sodium borohydride, MeOH / 2-methyl-propan-2-ol / 0.5 h / Heating

2: 41 percent / p-TsOH*H₂O / tetrahydrofuran / 0.5 h / Ambient temperature

3: 87 percent / CBr₄, PPh₃ / dimethylformamide / 0.5 h / 0 °C

4: 64 percent / K₂CO₃ / dimethylformamide / 5 h / Ambient temperature

With methanol; sodium tetrahydroborate; carbon tetrabromide; potassium carbonate; toluene-4-sulfonic acid; triphenylphosphine; In tetrahydrofuran; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1021/jm00392a020

Reference yield:

: 97845-58-4
5-(2-bromoethyl)-2,2-dimethyl-1,3-dioxane

: 127205-15-6
2-amino-6-benzyloxy-9-<2'-(2,2-dimethyl-1,3-dioxan-5-yl)-ethyl>-9H-purine

Guidance literature:: Multi-step reaction with 2 steps

1: 64 percent / K₂CO₃ / dimethylformamide / 5 h / Ambient temperature

With potassium carbonate; In N,N-dimethyl-formamide;
DOI:10.1021/jm00392a020