Ethanone, 1-(2-ethenyl-2-methylcyclobutyl)-, (1R-trans)- (9CI)

Base Information

Chemical Name:Ethanone, 1-(2-ethenyl-2-methylcyclobutyl)-, (1R-trans)- (9CI)
CAS No.:173829-77-1
Molecular Formula:C₉H₁₄O
Molecular Weight:138.21
Hs Code.:
Mol file:173829-77-1.mol

Synonyms:Ethanone, 1-(2-ethenyl-2-methylcyclobutyl)-, (1R-trans)- (9CI)

Suppliers and Price of Ethanone, 1-(2-ethenyl-2-methylcyclobutyl)-, (1R-trans)- (9CI)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Ethanone, 1-(2-ethenyl-2-methylcyclobutyl)-, (1R-trans)- (9CI)

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of Ethanone, 1-(2-ethenyl-2-methylcyclobutyl)-, (1R-trans)- (9CI)

There total 15 articles about Ethanone, 1-(2-ethenyl-2-methylcyclobutyl)-, (1R-trans)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 86994-12-9
2-methyl-1-(trimethylsilyl)cyclobutene

: 131510-64-0,173829-77-1,173829-76-0
1-acetyl-2-methyl-2-vinylcyclobutane

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) AlCl₃, 2.) 3N NaOH / 1.) CH₂Cl₂, 0 deg C

2: -78 -> 0 deg C

With sodium hydroxide; aluminium trichloride;
DOI:10.1021/ja00358a043

Reference yield:

: 67223-99-8
1-acetyl-2-methylcyclobutene

: 131510-64-0,173829-77-1,173829-76-0
1-acetyl-2-methyl-2-vinylcyclobutane

Guidance literature:: -78 -> 0 deg C;
DOI:10.1021/ja00358a043

Reference yield:

: 67223-99-8
1-acetyl-2-methylcyclobutene

: 917-57-7
vinyllithium

: 173829-77-1,173829-76-0
1-acetyl-2-methyl-2-vinylcyclobutane

: 173829-77-1,173829-76-0
1-acetyl-2-methyl-2-vinylcyclobutane

Guidance literature:: With CuCN; In tetrahydrofuran; diethyl ether; at -50 ℃; for 2.5h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
DOI:10.1021/ja00224a025