phenylbismuth(III) diacetate

Base Information

Chemical Name:phenylbismuth(III) diacetate
CAS No.:7205-03-0
Molecular Formula:C₁₀H₁₁BiO₄
Molecular Weight:404.175
Hs Code.:

Synonyms:phenylbismuth(III) diacetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of phenylbismuth(III) diacetate

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Technology Process of phenylbismuth(III) diacetate

There total 2 articles about phenylbismuth(III) diacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 603-33-8
triphenylbismuthane

: 64-19-7,77671-22-8
acetic acid

: 7205-03-0
phenylbismuth(III) diacetate

Guidance literature:: In diethyl ether; a soln. of acetic acid in ether was added to refluxing soln. of Ph3Bi in ether, mixt. was refluxed for 3 h at 32°C, mixt. was allowed tocool under N2; ppt. was collected; elem. anal.;

Reference yield:

: BiPh₃(OAc)2

: 22422-34-0
(1R,2R,3S,5R)-2,3-pinane diol

: 7205-03-0
phenylbismuth(III) diacetate

: 603-33-8
triphenylbismuthane

Guidance literature:: In dichloromethane-d2; byproducts: (CH3)2CC6H7CH3(OH)(OC6H5), C6H6, (CH3)2C4H4COCH3CH2COH; Irradiation (UV/VIS); under N2; an equimolar mixt. of Bi-contg. compd. and (-)-pinanediol in CD2Cl2 was refluxed at room temp.; irradn. (366 nm) after 12 h; (1)H NMR monitoring at room temp.;
DOI:10.1016/S0022-328X(02)01895-8