11-hydroxytetrahydrocarbazolenine

Base Information

• Chemical Name: 11-hydroxytetrahydrocarbazolenine
• CAS No.: 42738-99-8
• Molecular Formula: C₁₂H₁₃NO
• Molecular Weight: 187.241

Synonyms:11-hydroxytetrahydrocarbazolenine

Chemical Property of 11-hydroxytetrahydrocarbazolenine

Chemical Property:

Purity/Quality:

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Technology Process of 11-hydroxytetrahydrocarbazolenine

There total 2 articles about 11-hydroxytetrahydrocarbazolenine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.0%

1,2,3,4-tetrahydrocarbazole (942-01-8) → 11-hydroxytetrahydrocarbazolenine (42738-99-8) + o-phenol (78154-49-1) + spiro[cyclopentane-1,2'-indolin]-3'-one (4669-18-5)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at -60 ℃; for 0.833333h; further conditions;

Reference yield: 25.0%

1,2,3,4-tetrahydrocarbazole (942-01-8) + 3-chloro-benzenecarboperoxoic acid (937-14-4) → 11-hydroxytetrahydrocarbazolenine (42738-99-8) + o-phenol (78154-49-1) + spiro[cyclopentane-1,2'-indolin]-3'-one (4669-18-5)

Guidance literature:

In dichloromethane; at -60 ℃; for 0.833333h;

Reference yield: 90.0%

11-hydroxytetrahydrocarbazolenine (42738-99-8) + 2,6-dichlorobenzonitrile N-oxide (2904-62-3) → C19H16Cl2N2O2 (130872-84-3)

Guidance literature:

In chloroform; for 2h; Ambient temperature;

upstream raw materials:

1,2,3,4-tetrahydrocarbazole

3-chloro-benzenecarboperoxoic acid

Downstream raw materials:

2'-methylspiro[cyclopentane-1,3'-indole]

o-phenol

cyclohexane-1,2-dione

3-Chloro-N-(2-hydroxy-phenyl)-N-(6-oxo-cyclohex-1-enyl)-benzamide

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