benzyl 5-O-benzoyl-3-O-benzyl-2-O-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-β-D-ribofuranoside

Base Information

Chemical Name:benzyl 5-O-benzoyl-3-O-benzyl-2-O-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-β-D-ribofuranoside
CAS No.:93215-14-6
Molecular Formula:C₅₂H₄₆O₁₃
Molecular Weight:878.929
Hs Code.:

Synonyms:benzyl 5-O-benzoyl-3-O-benzyl-2-O-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-β-D-ribofuranoside

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Chemical Property of benzyl 5-O-benzoyl-3-O-benzyl-2-O-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-β-D-ribofuranoside

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Technology Process of benzyl 5-O-benzoyl-3-O-benzyl-2-O-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-β-D-ribofuranoside

There total 4 articles about benzyl 5-O-benzoyl-3-O-benzyl-2-O-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-β-D-ribofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 93245-41-1
benzyl 5-O-benzoyl-3-O-benzyl-β-D-ribofuranoside

: 22860-91-9
2,3,5-tri-O-benzoyl-D-ribofuranosyl bromide

: 93215-14-6
benzyl 5-O-benzoyl-3-O-benzyl-2-O-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-β-D-ribofuranoside

Guidance literature:: With calcium sulfate; silver trifluoromethanesulfonate; In dichloromethane; at -25 ℃; for 0.166667h;
DOI:10.1016/0008-6215(84)85223-4

Reference yield:

: 100-39-0
benzyl bromide

: 93215-14-6
benzyl 5-O-benzoyl-3-O-benzyl-2-O-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-β-D-ribofuranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) dibutyltin oxide / 1.) toluene, reflux, 3 h, 2.) N,N-dimethylformamide, 48 h, 70 deg C

2: 81 percent / silver triflate, Drierite / CH₂Cl₂ / 0.17 h / -25 °C

With calcium sulfate; silver trifluoromethanesulfonate; di(n-butyl)tin oxide; In dichloromethane;
DOI:10.1016/0008-6215(84)85223-4

Reference yield:

: 93215-12-4
benzyl 5-O-benzoyl-β-D-ribofuranoside

: 93215-14-6
benzyl 5-O-benzoyl-3-O-benzyl-2-O-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-β-D-ribofuranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) dibutyltin oxide / 1.) toluene, reflux, 3 h, 2.) N,N-dimethylformamide, 48 h, 70 deg C

2: 81 percent / silver triflate, Drierite / CH₂Cl₂ / 0.17 h / -25 °C

With calcium sulfate; silver trifluoromethanesulfonate; di(n-butyl)tin oxide; In dichloromethane;
DOI:10.1016/0008-6215(84)85223-4