Technology Process of C15H22N2O2
There total 4 articles about C15H22N2O2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
diethoxyphosphoryl-acetic acid ethyl ester;
With
sodium hydride;
In
tetrahydrofuran;
at 0 ℃;
for 1h;
1-(trans-4-methylcyclohexyl)-1H-imidazole-4-carbaldehyde;
In
tetrahydrofuran;
at 0 ℃;
for 1h;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: 4 h / 70 °C
2.1: lithium aluminium tetrahydride / tetrahydrofuran / 0.5 h / 0 °C
3.1: sodium hydrogencarbonate; iodine; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / water; toluene / 2 h / 20 °C
4.1: sodium hydride / tetrahydrofuran / 1 h / 0 °C
4.2: 1 h / 0 °C
With
lithium aluminium tetrahydride; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; iodine; sodium hydride; sodium hydrogencarbonate;
In
tetrahydrofuran; water; toluene;
4.1: |Wittig-Horner Reaction / 4.2: |Wittig-Horner Reaction;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: lithium aluminium tetrahydride / tetrahydrofuran / 0.5 h / 0 °C
2.1: sodium hydrogencarbonate; iodine; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / water; toluene / 2 h / 20 °C
3.1: sodium hydride / tetrahydrofuran / 1 h / 0 °C
3.2: 1 h / 0 °C
With
lithium aluminium tetrahydride; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; iodine; sodium hydride; sodium hydrogencarbonate;
In
tetrahydrofuran; water; toluene;
3.1: |Wittig-Horner Reaction / 3.2: |Wittig-Horner Reaction;