di(4-allyloxy)benzoylmethane

Base Information

Chemical Name:di(4-allyloxy)benzoylmethane
CAS No.:1262142-69-7
Molecular Formula:C₂₁H₂₀O₄
Molecular Weight:336.387
Hs Code.:

Synonyms:di(4-allyloxy)benzoylmethane

Suppliers and Price of di(4-allyloxy)benzoylmethane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of di(4-allyloxy)benzoylmethane

Chemical Property:

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Technology Process of di(4-allyloxy)benzoylmethane

There total 1 articles about di(4-allyloxy)benzoylmethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2079-53-0
1-(4-(allyloxy)phenyl)ethanone

: 35750-24-4
methyl 4-allyloxybenzoate

: 1262142-69-7
di(4-allyloxy)benzoylmethane

Guidance literature:: With sodium hydride; In tetrahydrofuran; for 48h; Reflux;
DOI:10.1039/c2jm32809g

Reference yield: 90.0%

: 1262142-69-7
di(4-allyloxy)benzoylmethane

: 109-63-7
boron trifluoride diethyl etherate

: 1393358-33-2
C₂₁H₁₉BF₂O₄

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 6h; Darkness;
DOI:10.1016/j.dyepig.2014.07.001

Reference yield: 67.0%

: 13798-24-8,19423-82-6
terbium(III) chloride hexahydrate

: 1262142-69-7
di(4-allyloxy)benzoylmethane

: [Tb₅(OH)5(di(4-allyloxy)benzoylmethanide)10]

Guidance literature:: With triethylamine; In methanol; byproducts: triethylammonium chloride; to soln. ligand in MeOH LnCl3*6H2O was added, stirred for 15 min, Et3N was added, heated at reflux for 16 h; volatiles were removed in vacuo, residue was triturated with toluene, filtered, concd. and pptd. with hexane; elem. anal.;
DOI:10.1039/c0dt00927j