((4S,4'S,5S,5'S)-2,2'-methylenebis(5-phenyl-4,5-dihydrooxazol-4,2-diyl))bis(methylene)dibenzoate

Base Information

Chemical Name:((4S,4'S,5S,5'S)-2,2'-methylenebis(5-phenyl-4,5-dihydrooxazol-4,2-diyl))bis(methylene)dibenzoate
CAS No.:1453106-66-5
Molecular Formula:C₃₅H₃₀N₂O₆
Molecular Weight:574.633
Hs Code.:

Synonyms:((4S,4'S,5S,5'S)-2,2'-methylenebis(5-phenyl-4,5-dihydrooxazol-4,2-diyl))bis(methylene)dibenzoate

Suppliers and Price of ((4S,4'S,5S,5'S)-2,2'-methylenebis(5-phenyl-4,5-dihydrooxazol-4,2-diyl))bis(methylene)dibenzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 2 raw suppliers

Chemical Property of ((4S,4'S,5S,5'S)-2,2'-methylenebis(5-phenyl-4,5-dihydrooxazol-4,2-diyl))bis(methylene)dibenzoate

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

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Technology Process of ((4S,4'S,5S,5'S)-2,2'-methylenebis(5-phenyl-4,5-dihydrooxazol-4,2-diyl))bis(methylene)dibenzoate

There total 4 articles about ((4S,4'S,5S,5'S)-2,2'-methylenebis(5-phenyl-4,5-dihydrooxazol-4,2-diyl))bis(methylene)dibenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 532-32-1
sodium benzoate

: 1453106-62-1
bis((4R,5S)-4-(bromomethyl)-5-phenyl-4,5-dihydrooxazol-2-yl)methane

: 1453106-66-5
((4S,4'S,5S,5'S)-2,2'-methylenebis(5-phenyl-4,5-dihydrooxazol-4,2-diyl))bis(methylene)dibenzoate

Guidance literature:: In dimethyl sulfoxide; at 50 ℃; for 12h; Inert atmosphere; Schlenk technique; Sealed tube;
DOI:10.1002/ejoc.201300279

Reference yield:

: 10344-69-1
diethyl malonoimidate dihydrochloride

: 1453106-66-5
((4S,4'S,5S,5'S)-2,2'-methylenebis(5-phenyl-4,5-dihydrooxazol-4,2-diyl))bis(methylene)dibenzoate

Guidance literature:: Multi-step reaction with 3 steps

1: dichloromethane / 18 h / Inert atmosphere; Schlenk technique; Reflux

2: carbon tetrabromide; triphenylphosphine / dichloromethane / 16 h / 20 °C / Inert atmosphere; Schlenk technique

3: dimethyl sulfoxide / 12 h / 50 °C / Inert atmosphere; Schlenk technique; Sealed tube

With carbon tetrabromide; triphenylphosphine; In dichloromethane; dimethyl sulfoxide;
DOI:10.1002/ejoc.201300279

Reference yield:

: 133463-87-3
(-)-(4S,4'S,5S,5'S)-4,4',5,5'-Tetrahydro-2,2'-methylene-5,5'-diphenylbis-4,4'-di(methanol)

: 1453106-66-5
((4S,4'S,5S,5'S)-2,2'-methylenebis(5-phenyl-4,5-dihydrooxazol-4,2-diyl))bis(methylene)dibenzoate

Guidance literature:: Multi-step reaction with 2 steps

1: carbon tetrabromide; triphenylphosphine / dichloromethane / 16 h / 20 °C / Inert atmosphere; Schlenk technique

2: dimethyl sulfoxide / 12 h / 50 °C / Inert atmosphere; Schlenk technique; Sealed tube

With carbon tetrabromide; triphenylphosphine; In dichloromethane; dimethyl sulfoxide;
DOI:10.1002/ejoc.201300279