C₂₃H₃₄SiO₂

Base Information

• Chemical Name: C₂₃H₃₄SiO₂
• CAS No.: 946409-00-3
• Molecular Formula: C₂₃H₃₄O₂Si
• Molecular Weight: 370.607
• Mol file: 946409-00-3.mol

Synonyms:C₂₃H₃₄SiO₂

Chemical Property of C₂₃H₃₄SiO₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of C₂₃H₃₄SiO₂

There total 1 articles about C₂₃H₃₄SiO₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

(5S)-2-methyl-1,5-hexanediol + tert-butylchlorodiphenylsilane (58479-61-1) → C23H34SiO2 (946409-00-3)

Guidance literature:

With 1H-imidazole; In N,N-dimethyl-formamide; at 23 ℃; for 3h;

DOI:10.1021/ol0707259

Reference yield:

C23H34SiO2 (946409-00-3) + methanesulfonyl chloride (124-63-0) → C24H36SiO4S

Guidance literature:

With dmap; triethylamine; In dichloromethane; at 23 ℃; for 3h;

DOI:10.1021/ol0707259

Reference yield:

C23H34SiO2 (946409-00-3) → (2R)-1-tert-butyldiphenylsilyloxy-2-methyl-hexane (946408-99-7)

Guidance literature:

Multi-step reaction with 2 steps

1: dmap; triethylamine / dichloromethane / 3 h / 23 °C

2: lithium aluminium tetrahydride / diethyl ether / 23 °C

With dmap; lithium aluminium tetrahydride; triethylamine; In diethyl ether; dichloromethane;

DOI:10.1021/ol0707259

upstream raw materials:

tert-butylchlorodiphenylsilane

Downstream raw materials:

(2R)-1-tert-butyldiphenylsilyloxy-2-methyl-hexane

(2S)-2-methyl-1-hexanol

(2R)-methyl-1-hexanol