1-butyl-3-(3-formyl-4-hydroxybenzyl)-1H-imidazol-3-ium chloride

Base Information

• Chemical Name: 1-butyl-3-(3-formyl-4-hydroxybenzyl)-1H-imidazol-3-ium chloride
• CAS No.: 1580445-91-5
• Molecular Formula: C₁₅H₁₉N₂O₂*Cl
• Molecular Weight: 294.781
• Mol file: 1580445-91-5.mol

Synonyms:1-butyl-3-(3-formyl-4-hydroxybenzyl)-1H-imidazol-3-ium chloride

Chemical Property of 1-butyl-3-(3-formyl-4-hydroxybenzyl)-1H-imidazol-3-ium chloride

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-butyl-3-(3-formyl-4-hydroxybenzyl)-1H-imidazol-3-ium chloride

There total 3 articles about 1-butyl-3-(3-formyl-4-hydroxybenzyl)-1H-imidazol-3-ium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

1-Butylimidazole (4316-42-1) + 5-(chloromethyl)salicylaldehyde (23731-06-8) → 1-butyl-3-(3-formyl-4-hydroxybenzyl)-1H-imidazol-3-ium chloride (1580445-91-5)

Guidance literature:

In toluene; at 20 - 60 ℃; for 24h; Inert atmosphere;

DOI:10.1016/j.ejmech.2013.09.029

Reference yield:

salicylaldehyde (90-02-8) → 1-butyl-3-(3-formyl-4-hydroxybenzyl)-1H-imidazol-3-ium chloride (1580445-91-5)

Guidance literature:

Multi-step reaction with 2 steps

1: hydrogenchloride; zinc(II) chloride / water / 24 h / 20 °C

2: toluene / 24 h / 20 - 60 °C / Inert atmosphere

With hydrogenchloride; zinc(II) chloride; In water; toluene;

DOI:10.1016/j.ejmech.2013.09.029

Reference yield:

phenol (108-95-2,27073-41-2) → 1-butyl-3-(3-formyl-4-hydroxybenzyl)-1H-imidazol-3-ium chloride (1580445-91-5)

Guidance literature:

Multi-step reaction with 3 steps

1: magnesium chloride; triethylamine / acetonitrile / 20 °C

2: hydrogenchloride; zinc(II) chloride / water / 24 h / 20 °C

3: toluene / 24 h / 20 - 60 °C / Inert atmosphere

With hydrogenchloride; triethylamine; magnesium chloride; zinc(II) chloride; In water; toluene; acetonitrile;

DOI:10.1016/j.ejmech.2013.09.029

upstream raw materials:

phenol

1-Butylimidazole

5-(chloromethyl)salicylaldehyde

salicylaldehyde