.alpha.-D-Glucopyranoside, methyl 6-deoxy-6-iodo-, 4-acetate 3-benzoate 2-(4-methylbenzenesulfonate)

Base Information

Chemical Name:.alpha.-D-Glucopyranoside, methyl 6-deoxy-6-iodo-, 4-acetate 3-benzoate 2-(4-methylbenzenesulfonate)
CAS No.:165375-11-1
Molecular Formula:C23H25 I O9 S
Molecular Weight:604.41
Hs Code.:

Synonyms:.alpha.-D-Glucopyranoside, methyl 6-deoxy-6-iodo-, 4-acetate 3-benzoate 2-(4-methylbenzenesulfonate)

Suppliers and Price of .alpha.-D-Glucopyranoside, methyl 6-deoxy-6-iodo-, 4-acetate 3-benzoate 2-(4-methylbenzenesulfonate)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of .alpha.-D-Glucopyranoside, methyl 6-deoxy-6-iodo-, 4-acetate 3-benzoate 2-(4-methylbenzenesulfonate)

Chemical Property:

Boiling Point:652.7±55.0 °C(Predicted)
PSA：122.81000
Density:1.60±0.1 g/cm3(Predicted)
LogP:4.11330

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of .alpha.-D-Glucopyranoside, methyl 6-deoxy-6-iodo-, 4-acetate 3-benzoate 2-(4-methylbenzenesulfonate)

There total 4 articles about .alpha.-D-Glucopyranoside, methyl 6-deoxy-6-iodo-, 4-acetate 3-benzoate 2-(4-methylbenzenesulfonate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 165375-10-0
methyl 4-O-acetyl-3-O-benzoyl-2,6-di-O-tosyl-α-D-glucopyranoside

: 165375-11-1
methyl 4-O-acetyl-3-O-benzoyl-6-deoxy-6-iodo-2-O-tosyl-α-D-glucopyranoside

Guidance literature:: With sodium iodide; In acetic anhydride; for 1h; Heating;

Reference yield:

: 54497-89-1
methyl 2,6-bis-α-D-glucopyranoside

: 165375-11-1
methyl 4-O-acetyl-3-O-benzoyl-6-deoxy-6-iodo-2-O-tosyl-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 55 percent / pyridine / 1.) 0 deg C, 7 h, 2.) 20 deg C, 30 h

2: 86 percent / pyridine / 1 h / 20 °C

3: 83 percent / NaI / acetic anhydride / 1 h / Heating

With sodium iodide; In pyridine; acetic anhydride;

Reference yield:

: 98-88-4
benzoyl chloride

: 165375-11-1
methyl 4-O-acetyl-3-O-benzoyl-6-deoxy-6-iodo-2-O-tosyl-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 55 percent / pyridine / 1.) 0 deg C, 7 h, 2.) 20 deg C, 30 h

2: 86 percent / pyridine / 1 h / 20 °C

3: 83 percent / NaI / acetic anhydride / 1 h / Heating

With sodium iodide; In pyridine; acetic anhydride;