phenyl N-{[(2-hydroxypropyl)[(4-methoxyphenyl)methyl]carbamoyl]methyl}-N-methylcarbamate

Base Information

Chemical Name:phenyl N-{[(2-hydroxypropyl)[(4-methoxyphenyl)methyl]carbamoyl]methyl}-N-methylcarbamate
CAS No.:1375744-89-0
Molecular Formula:C₂₁H₂₆N₂O₅
Molecular Weight:386.448
Hs Code.:

Synonyms:phenyl N-{[(2-hydroxypropyl)[(4-methoxyphenyl)methyl]carbamoyl]methyl}-N-methylcarbamate

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Chemical Property of phenyl N-{[(2-hydroxypropyl)[(4-methoxyphenyl)methyl]carbamoyl]methyl}-N-methylcarbamate

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Technology Process of phenyl N-{[(2-hydroxypropyl)[(4-methoxyphenyl)methyl]carbamoyl]methyl}-N-methylcarbamate

There total 3 articles about phenyl N-{[(2-hydroxypropyl)[(4-methoxyphenyl)methyl]carbamoyl]methyl}-N-methylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 1096711-35-1
phenyl (2-chloro-2-oxoethyl)methylcarbamate

: 856978-80-8
1-{[(4-methoxyphenyl)methyl]amino}propan-2-ol

: 1375744-89-0
phenyl N-{[(2-hydroxypropyl)[(4-methoxyphenyl)methyl]carbamoyl]methyl}-N-methylcarbamate

Guidance literature:: With sodium hydrogencarbonate; In tetrahydrofuran; 1,4-dioxane; water; at 0 ℃;
DOI:10.1021/jo3007144

Reference yield:

: 754145-88-5
C₁₁H₁₅NO₂

: 1375744-89-0
phenyl N-{[(2-hydroxypropyl)[(4-methoxyphenyl)methyl]carbamoyl]methyl}-N-methylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium cyanoborohydride / tetrahydrofuran / Cooling with ice

2: sodium hydrogencarbonate / tetrahydrofuran; 1,4-dioxane; water / 0 °C

With sodium cyanoborohydride; sodium hydrogencarbonate; In tetrahydrofuran; 1,4-dioxane; water;
DOI:10.1021/jo3007144

Reference yield:

: 123-11-5
4-methoxy-benzaldehyde

: 1375744-89-0
phenyl N-{[(2-hydroxypropyl)[(4-methoxyphenyl)methyl]carbamoyl]methyl}-N-methylcarbamate

Guidance literature:: Multi-step reaction with 3 steps

1: acetic acid / tetrahydrofuran / 1 h / 0 - 20 °C

2: sodium cyanoborohydride / tetrahydrofuran / Cooling with ice

3: sodium hydrogencarbonate / tetrahydrofuran; 1,4-dioxane; water / 0 °C

With sodium cyanoborohydride; sodium hydrogencarbonate; acetic acid; In tetrahydrofuran; 1,4-dioxane; water;
DOI:10.1021/jo3007144