Technology Process of C60H52BN3O2
There total 4 articles about C60H52BN3O2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
[1,1'-bis(diphenylphosphino)ferrocene]dichloropalladium(II); potassium acetate;
In
1,4-dioxane;
at 85 ℃;
Inert atmosphere;
Large scale reaction;
DOI:10.1021/cm202732j
- Guidance literature:
-
Multi-step reaction with 3 steps
1: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / water; toluene / 48 h / 110 °C / Inert atmosphere
2: copper(l) iodide; trans-1,2-Diaminocyclohexane; potassium tert-butylate / 1,4-dioxane / 110 °C / Inert atmosphere; Large scale reaction
3: [1,1'-bis(diphenylphosphino)ferrocene]dichloropalladium(II); potassium acetate / 1,4-dioxane / 85 °C / Inert atmosphere; Large scale reaction
With
copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); [1,1'-bis(diphenylphosphino)ferrocene]dichloropalladium(II); trans-1,2-Diaminocyclohexane; potassium tert-butylate; potassium acetate; sodium carbonate;
In
1,4-dioxane; water; toluene;
1: Suzuki coupling;
DOI:10.1021/cm202732j
- Guidance literature:
-
Multi-step reaction with 3 steps
1: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / water; toluene / 48 h / 110 °C / Inert atmosphere
2: copper(l) iodide; trans-1,2-Diaminocyclohexane; potassium tert-butylate / 1,4-dioxane / 110 °C / Inert atmosphere; Large scale reaction
3: [1,1'-bis(diphenylphosphino)ferrocene]dichloropalladium(II); potassium acetate / 1,4-dioxane / 85 °C / Inert atmosphere; Large scale reaction
With
copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); [1,1'-bis(diphenylphosphino)ferrocene]dichloropalladium(II); trans-1,2-Diaminocyclohexane; potassium tert-butylate; potassium acetate; sodium carbonate;
In
1,4-dioxane; water; toluene;
1: Suzuki coupling;
DOI:10.1021/cm202732j