N-(4-phenoxybenzenesulfonyl)-N-tert-butoxycarbonylmethyl-O-benzyl-D-valinehydroxamic acid

Base Information

Chemical Name:N-(4-phenoxybenzenesulfonyl)-N-tert-butoxycarbonylmethyl-O-benzyl-D-valinehydroxamic acid
CAS No.:1092690-93-1
Molecular Formula:C₃₀H₃₆N₂O₇S
Molecular Weight:568.691
Hs Code.:

Synonyms:N-(4-phenoxybenzenesulfonyl)-N-tert-butoxycarbonylmethyl-O-benzyl-D-valinehydroxamic acid

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Chemical Property of N-(4-phenoxybenzenesulfonyl)-N-tert-butoxycarbonylmethyl-O-benzyl-D-valinehydroxamic acid

Chemical Property:

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Technology Process of N-(4-phenoxybenzenesulfonyl)-N-tert-butoxycarbonylmethyl-O-benzyl-D-valinehydroxamic acid

There total 8 articles about N-(4-phenoxybenzenesulfonyl)-N-tert-butoxycarbonylmethyl-O-benzyl-D-valinehydroxamic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₆H₃₃NO₉S

: 2687-43-6
O-benzylhydoxylamine hydrochloride

: 1092690-93-1
N-(4-phenoxybenzenesulfonyl)-N-tert-butoxycarbonylmethyl-O-benzyl-D-valinehydroxamic acid

Guidance literature:: O-benzylhydoxylamine hydrochloride; With potassium hydroxide; In methanol; at 0 ℃; for 0.5h;

C₂₆H₃₃NO₉S; In tetrahydrofuran; methanol; at 0 ℃; Inert atmosphere;
DOI:10.1021/jm800964f

Reference yield:

: 1092690-90-8
N-(4-phenoxybenzenesulfonyl)-N-tert-butoxycarbonylmethyl-D-valine

: 1092690-93-1
N-(4-phenoxybenzenesulfonyl)-N-tert-butoxycarbonylmethyl-O-benzyl-D-valinehydroxamic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 4-methyl-morpholine / tetrahydrofuran / 0 °C

2: methanol / 0 °C

With 4-methyl-morpholine; In tetrahydrofuran; methanol;
DOI:10.1021/jm200593b

Reference yield:

: 1092690-85-1
N-(4-phenoxybenzenesulfonyl)-O-benzyl-D-valine

: 1092690-93-1
N-(4-phenoxybenzenesulfonyl)-N-tert-butoxycarbonylmethyl-O-benzyl-D-valinehydroxamic acid

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 20 °C

2: palladium 10% on activated carbon; hydrogen / methanol / 20 °C

3: 4-methyl-morpholine / tetrahydrofuran / 0 °C

4: methanol / 0 °C

With 4-methyl-morpholine; palladium 10% on activated carbon; hydrogen; potassium carbonate; potassium iodide; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;
DOI:10.1021/jm200593b