4-Iodo-1-tosyl-1H-imidazole

Base Information

Chemical Name:4-Iodo-1-tosyl-1H-imidazole
CAS No.:163854-63-5
Molecular Formula:C10H9 I N2 O2 S
Molecular Weight:348.164
Hs Code.:2933290090
DSSTox Substance ID:DTXSID10392246
Nikkaji Number:J1.584.405A
Wikidata:Q82190308
Mol file:163854-63-5.mol

Synonyms:4-IODO-1-TOSYL-1H-IMIDAZOLE;163854-63-5;4-Iodo-1-p-tosylimidazole;4-iodo-1-(4-methylphenyl)sulfonylimidazole;4-Iodo-1-[(4-methylphenyl)sulfonyl]-1H-imidazole;1H-Imidazole, 4-iodo-1-[(4-methylphenyl)sulfonyl]-;4-iodo-1-(4-methylbenzenesulfonyl)-1H-imidazole;1-Tosyl-4-iodo-1H-imidazole;SCHEMBL14973039;DTXSID10392246;GNMAMHYZZVUENR-UHFFFAOYSA-N;MFCD04039580;AKOS015853971;CS-0212398;FT-0670396;A882533;J-010096

Suppliers and Price of 4-Iodo-1-tosyl-1H-imidazole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
4-Iodo-1-p-tosylimidazole
5g
$ 595.00

TRC
4-Iodo-1-p-tosylimidazole
10g
$ 970.00

TRC
4-Iodo-1-p-tosylimidazole
2g
$ 250.00

Medical Isotopes, Inc.
4-Iodo-1-p-tosylimidazole
5 g
$ 1560.00

Medical Isotopes, Inc.
4-Iodo-1-p-tosylimidazole
1 g
$ 820.00

Crysdot
4-Iodo-1-tosyl-1H-imidazole 95+%
25g
$ 456.00

Chemenu
4-Iodo-1-tosyl-1H-imidazole 95%
25g
$ 426.00

American Custom Chemicals Corporation
4-IODO-1-P-TOSYLIMIDAZOLE 95.00%
10G
$ 2055.90

American Custom Chemicals Corporation
4-IODO-1-P-TOSYLIMIDAZOLE 95.00%
1G
$ 716.10

Alichem
4-Iodo-1-tosyl-1H-imidazole
25g
$ 460.56

Total 12 raw suppliers

Chemical Property of 4-Iodo-1-tosyl-1H-imidazole

Chemical Property:

Vapor Pressure:2.67E-09mmHg at 25°C
Melting Point:147-148°C
Refractive Index:1.695
Boiling Point:478°C at 760 mmHg
Flash Point:242.9°C
PSA：60.34000
Density:1.84g/cm³
LogP:3.11390
XLogP3:2.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:347.94295
Heavy Atom Count:16
Complexity:333

Purity/Quality:

97% ^*data from raw suppliers

4-Iodo-1-p-tosylimidazole ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC=C(C=C1)S(=O)(=O)N2C=C(N=C2)I
Uses Imidazole rings are found in numberous natural compounds such as enzymes, nucleic acid, and alkaloids that play a role in biological processes Imidazole rings are found in numberous natural compounds such as enzymes, nucleic acid, and alkaloids that play a role in biological processes.

Technology Process of 4-Iodo-1-tosyl-1H-imidazole

There total 1 articles about 4-Iodo-1-tosyl-1H-imidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 71759-89-2
4-iodoimidazole

: 98-59-9
p-toluenesulfonyl chloride

: 163854-63-5
4-iodo-1-[(4-methylphenyl)sulfonyl]-1H-imidazole

Guidance literature:: With triethylamine; In tetrahydrofuran; for 24h;
DOI:10.1021/jo00113a016

Reference yield: 99.0%

: 76782-82-6
tert-Butyldimethyl(prop-2-ynyloxy)silane

: 163854-63-5
4-iodo-1-[(4-methylphenyl)sulfonyl]-1H-imidazole

: N-tosyl-4-[3-(tert-butyldimethylsiloxy)prop-1-ynyl]imidazole

Guidance literature:: With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine; In N,N-dimethyl-formamide; at 80 ℃; for 0.5h; Microwave irradiation; Sealed tube; Inert atmosphere;
DOI:10.1002/ejoc.201500520

Reference yield: 95.0%

: 78592-82-2
4-(tert-butyldimethylsilyloxy)-1-butyne

: 163854-63-5
4-iodo-1-[(4-methylphenyl)sulfonyl]-1H-imidazole

: N-tosyl-4-[3-(tert-butyldimethylsiloxy)but-1-ynyl]imidazole

Guidance literature:: With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine; In N,N-dimethyl-formamide; at 80 ℃; for 0.5h; Microwave irradiation; Sealed tube; Inert atmosphere;
DOI:10.1002/ejoc.201500520