(S)-3-Methyl-2-[methyl-(7-octyl-1H-indol-4-yl)-amino]-butyric acid benzyl ester

Base Information

Chemical Name:(S)-3-Methyl-2-[methyl-(7-octyl-1H-indol-4-yl)-amino]-butyric acid benzyl ester
CAS No.:160096-22-0
Molecular Formula:C₂₉H₄₀N₂O₂
Molecular Weight:448.649
Hs Code.:

Synonyms:(S)-3-Methyl-2-[methyl-(7-octyl-1H-indol-4-yl)-amino]-butyric acid benzyl ester

Suppliers and Price of (S)-3-Methyl-2-[methyl-(7-octyl-1H-indol-4-yl)-amino]-butyric acid benzyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of (S)-3-Methyl-2-[methyl-(7-octyl-1H-indol-4-yl)-amino]-butyric acid benzyl ester

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of (S)-3-Methyl-2-[methyl-(7-octyl-1H-indol-4-yl)-amino]-butyric acid benzyl ester

There total 7 articles about (S)-3-Methyl-2-[methyl-(7-octyl-1H-indol-4-yl)-amino]-butyric acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4769-97-5
4-nitro-1H-indoIe

: 160096-22-0
(S)-3-Methyl-2-[methyl-(7-octyl-1H-indol-4-yl)-amino]-butyric acid benzyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 27 percent / tetrahydrofuran / 0 °C

2: hydrogen / Pd-C

3: tetrahydrofuran

4: BH₃-Me₂S / tetrahydrofuran / 60 °C

5: 2,6-lutidine / 1,2-dichloro-ethane / 95 °C

With 2,6-dimethylpyridine; dimethylsulfide borane complex; hydrogen; palladium on activated charcoal; In tetrahydrofuran; 1,2-dichloro-ethane;
DOI:10.1016/S0040-4039(00)78434-6

Reference yield:

: 62331-02-6
N'-(2-methyl-3-nitrophenyl)-N,N-dimethylformamidine

: 160096-22-0
(S)-3-Methyl-2-[methyl-(7-octyl-1H-indol-4-yl)-amino]-butyric acid benzyl ester

Guidance literature:: Multi-step reaction with 6 steps

1: potassium ethoxide/diethyl oxalate / tetrahydrofuran

2: 27 percent / tetrahydrofuran / 0 °C

3: hydrogen / Pd-C

4: tetrahydrofuran

5: BH₃-Me₂S / tetrahydrofuran / 60 °C

6: 2,6-lutidine / 1,2-dichloro-ethane / 95 °C

With 2,6-dimethylpyridine; dimethylsulfide borane complex; potassium ethoxide; hydrogen; oxalic acid diethyl ester; palladium on activated charcoal; In tetrahydrofuran; 1,2-dichloro-ethane;
DOI:10.1016/S0040-4039(00)78434-6

Reference yield:

: 38841-98-4
n-octylmagnesium chloride

: 160096-22-0
(S)-3-Methyl-2-[methyl-(7-octyl-1H-indol-4-yl)-amino]-butyric acid benzyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 27 percent / tetrahydrofuran / 0 °C

2: hydrogen / Pd-C

3: tetrahydrofuran

4: BH₃-Me₂S / tetrahydrofuran / 60 °C

5: 2,6-lutidine / 1,2-dichloro-ethane / 95 °C

With 2,6-dimethylpyridine; dimethylsulfide borane complex; hydrogen; palladium on activated charcoal; In tetrahydrofuran; 1,2-dichloro-ethane;
DOI:10.1016/S0040-4039(00)78434-6