(4-{benzyl[2-(bis-pyridin-2-ylmethylamino)ethyl]amino}-2-oxobutyl)carbamic acid tert-butyl ester

Base Information

Chemical Name:(4-{benzyl[2-(bis-pyridin-2-ylmethylamino)ethyl]amino}-2-oxobutyl)carbamic acid tert-butyl ester
CAS No.:402921-67-9
Molecular Formula:C₃₀H₃₉N₅O₃
Molecular Weight:517.671
Hs Code.:

Synonyms:(4-{benzyl[2-(bis-pyridin-2-ylmethylamino)ethyl]amino}-2-oxobutyl)carbamic acid tert-butyl ester

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Chemical Property of (4-{benzyl[2-(bis-pyridin-2-ylmethylamino)ethyl]amino}-2-oxobutyl)carbamic acid tert-butyl ester

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Technology Process of (4-{benzyl[2-(bis-pyridin-2-ylmethylamino)ethyl]amino}-2-oxobutyl)carbamic acid tert-butyl ester

There total 10 articles about (4-{benzyl[2-(bis-pyridin-2-ylmethylamino)ethyl]amino}-2-oxobutyl)carbamic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 121505-96-2
(2-oxobut-3-enyl)carbamic acid tert-butyl ester

: 402921-64-6
N-benzyl-N’,N’-bis(2-pyridylmethyl)-1,2-diaminoethane

: 402921-67-9
(4-{benzyl[2-(bis-pyridin-2-ylmethylamino)ethyl]amino}-2-oxobutyl)carbamic acid tert-butyl ester

Guidance literature:: In methanol; at 20 ℃; for 18h;
DOI:10.1039/b103164n

Reference yield:

: 189440-33-3
(2-aminoethyl)bis(2-pyridylmethyl)amine

: 402921-67-9
(4-{benzyl[2-(bis-pyridin-2-ylmethylamino)ethyl]amino}-2-oxobutyl)carbamic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / MgSO₄ / CH₂Cl₂ / 3 h / 20 °C

2: 91 percent / NaBH₄ / acetonitrile; acetic acid; ethanol / 18 h / 20 °C

3: 100 percent / methanol / 18 h / 20 °C

With sodium tetrahydroborate; magnesium sulfate; In methanol; ethanol; dichloromethane; acetic acid; acetonitrile; 3: Michael addition;
DOI:10.1039/b103164n

Reference yield:

: 1121-60-4
pyridine-2-carbaldehyde

: 402921-67-9
(4-{benzyl[2-(bis-pyridin-2-ylmethylamino)ethyl]amino}-2-oxobutyl)carbamic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 7 steps

1: 100 percent / MgSO₄ / CH₂Cl₂ / 3 h / 20 °C

2: 73 percent / NaBH₄ / acetonitrile; ethanol; acetic acid / 18 h / 20 °C

3: 68 percent / K₂CO₃; KI / acetonitrile / 24 h / Heating

4: 68 percent / hydrazine monohydrate / ethanol / 3 h / Heating

5: 100 percent / MgSO₄ / CH₂Cl₂ / 3 h / 20 °C

6: 91 percent / NaBH₄ / acetonitrile; acetic acid; ethanol / 18 h / 20 °C

7: 100 percent / methanol / 18 h / 20 °C

With sodium tetrahydroborate; magnesium sulfate; potassium carbonate; hydrazine hydrate; potassium iodide; In methanol; ethanol; dichloromethane; acetic acid; acetonitrile; 7: Michael addition;
DOI:10.1039/b103164n