7,18-Bis(benzyloxy)-1-(tert-butoxycarbonyl)-8,11-dioxo-1,7,12,18-tetraazaoctadecane

Base Information

Chemical Name:7,18-Bis(benzyloxy)-1-(tert-butoxycarbonyl)-8,11-dioxo-1,7,12,18-tetraazaoctadecane
CAS No.:160388-22-7
Molecular Formula:C₃₃H₅₀N₄O₆
Molecular Weight:598.783
Hs Code.:

Synonyms:7,18-Bis(benzyloxy)-1-(tert-butoxycarbonyl)-8,11-dioxo-1,7,12,18-tetraazaoctadecane

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Chemical Property of 7,18-Bis(benzyloxy)-1-(tert-butoxycarbonyl)-8,11-dioxo-1,7,12,18-tetraazaoctadecane

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Technology Process of 7,18-Bis(benzyloxy)-1-(tert-butoxycarbonyl)-8,11-dioxo-1,7,12,18-tetraazaoctadecane

There total 6 articles about 7,18-Bis(benzyloxy)-1-(tert-butoxycarbonyl)-8,11-dioxo-1,7,12,18-tetraazaoctadecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 129245-21-2
O-benzyl-N-(5-aminopentyl)-N-(tert-butoxycarbonyl)hydroxylamine

: 160388-22-7
7,18-Bis(benzyloxy)-1-(tert-butoxycarbonyl)-8,11-dioxo-1,7,12,18-tetraazaoctadecane

Guidance literature:: Multi-step reaction with 5 steps

1: TFA / CH₂Cl₂ / 30 h / Ambient temperature

2: tetrahydrofuran / 24 h

3: 88 percent / pyridine / 1.5 h / 80 - 86 °C

4: CH₂Cl₂ / 1 h

5: CH₂Cl₂ / 12 h

With pyridine; trifluoroacetic acid; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo00106a022

Reference yield:

: 58632-95-4
2-(tert-Butoxycarbonyloxyimino)-2-phenylacetonitrile

: 160388-22-7
7,18-Bis(benzyloxy)-1-(tert-butoxycarbonyl)-8,11-dioxo-1,7,12,18-tetraazaoctadecane

Guidance literature:: Multi-step reaction with 4 steps

1: tetrahydrofuran / 24 h

2: 88 percent / pyridine / 1.5 h / 80 - 86 °C

3: CH₂Cl₂ / 1 h

4: CH₂Cl₂ / 12 h

With pyridine; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo00106a022

Reference yield:

: 160388-21-6
N-(Benzyloxy)-1,5-pentanediamine

: 160388-22-7
7,18-Bis(benzyloxy)-1-(tert-butoxycarbonyl)-8,11-dioxo-1,7,12,18-tetraazaoctadecane

Guidance literature:: Multi-step reaction with 4 steps

1: tetrahydrofuran / 24 h

2: 88 percent / pyridine / 1.5 h / 80 - 86 °C

3: CH₂Cl₂ / 1 h

4: CH₂Cl₂ / 12 h

With pyridine; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo00106a022