diethyl tert-butoxycarbonylamino-2-(3,5-diiodo-4-hydroxyphenyl)ethylphosphonate

Base Information

Chemical Name:diethyl tert-butoxycarbonylamino-2-(3,5-diiodo-4-hydroxyphenyl)ethylphosphonate
CAS No.:852947-21-8
Molecular Formula:C₁₇H₂₆I₂NO₆P
Molecular Weight:625.179
Hs Code.:

Synonyms:diethyl tert-butoxycarbonylamino-2-(3,5-diiodo-4-hydroxyphenyl)ethylphosphonate

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Chemical Property of diethyl tert-butoxycarbonylamino-2-(3,5-diiodo-4-hydroxyphenyl)ethylphosphonate

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Technology Process of diethyl tert-butoxycarbonylamino-2-(3,5-diiodo-4-hydroxyphenyl)ethylphosphonate

There total 7 articles about diethyl tert-butoxycarbonylamino-2-(3,5-diiodo-4-hydroxyphenyl)ethylphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₇H₂₈NO₆P

: 852947-21-8
diethyl tert-butoxycarbonylamino-2-(3,5-diiodo-4-hydroxyphenyl)ethylphosphonate

Guidance literature:: With [bis(pyridine)iodine]⁺ tetrafluoroborate; In chloroform; at 20 ℃; for 1h;

Reference yield:

: 91726-12-4,84891-34-9
diethyl 1-amino-2-(4-benzyloxyphenyl)ethyl phosphonate

: 852947-21-8
diethyl tert-butoxycarbonylamino-2-(3,5-diiodo-4-hydroxyphenyl)ethylphosphonate

Guidance literature:: Multi-step reaction with 3 steps

1: tetrahydrofuran / 4 h / Heating / reflux

2: hydrogen / palladium 10% on activated carbon / methanol / 16 h

3: [bis(pyridine)iodine]⁺ tetrafluoroborate / dichloromethane / 1 h / 20 °C

With hydrogen; [bis(pyridine)iodine]⁺ tetrafluoroborate; palladium 10% on activated carbon; In tetrahydrofuran; methanol; dichloromethane;

Reference yield:

: 84891-33-8
diethyl 2-(4-benzyloxyphenyl)-1-hydroxyiminoethylphosphonate

: 852947-21-8
diethyl tert-butoxycarbonylamino-2-(3,5-diiodo-4-hydroxyphenyl)ethylphosphonate

Guidance literature:: Multi-step reaction with 5 steps

1: sodium tetrahydroborate / nickel dichloride / methanol / 16 h / 20 °C

2: potassium hydroxide; water

3: tetrahydrofuran / 4 h / Heating / reflux

4: hydrogen / palladium 10% on activated carbon / methanol / 16 h

5: [bis(pyridine)iodine]⁺ tetrafluoroborate / dichloromethane / 1 h / 20 °C

With potassium hydroxide; sodium tetrahydroborate; water; hydrogen; [bis(pyridine)iodine]⁺ tetrafluoroborate; palladium 10% on activated carbon; nickel dichloride; In tetrahydrofuran; methanol; dichloromethane;