methyl [4,6-dihydroxy-2-(4-nitrobenzyl)-[2-(13C)]pyrimidin-5-yl]acetate

Base Information

Chemical Name:methyl [4,6-dihydroxy-2-(4-nitrobenzyl)-[2-(13C)]pyrimidin-5-yl]acetate
CAS No.:1214271-97-2
Molecular Formula:C₁₄H₁₃N₃O₆
Molecular Weight:320.263
Hs Code.:

Synonyms:methyl [4,6-dihydroxy-2-(4-nitrobenzyl)-[2-(13C)]pyrimidin-5-yl]acetate

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Chemical Property of methyl [4,6-dihydroxy-2-(4-nitrobenzyl)-[2-(13C)]pyrimidin-5-yl]acetate

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Technology Process of methyl [4,6-dihydroxy-2-(4-nitrobenzyl)-[2-(13C)]pyrimidin-5-yl]acetate

There total 4 articles about methyl [4,6-dihydroxy-2-(4-nitrobenzyl)-[2-(13C)]pyrimidin-5-yl]acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 67-56-1
methanol

: 7459-46-3
triethyl 1,1,2-ethanetricarboxylate

: 1214271-96-1
2-(4-nitrophenyl)-[1-(13C)]ethanimidamide hydrochloride

: 1214271-97-2
methyl [4,6-dihydroxy-2-(4-nitrobenzyl)-[2-(13C)]pyrimidin-5-yl]acetate

Guidance literature:: methanol; triethyl 1,1,2-ethanetricarboxylate; 2-(4-nitrophenyl)-[1-(13C)]ethanimidamide hydrochloride; With sodium methylate; In methanol; for 1.5h; Reflux;

With hydrogenchloride; water; In methanol; at 0 ℃; for 0.5h;

Reference yield:

: 100-39-0
benzyl bromide

: 1214271-97-2
methyl [4,6-dihydroxy-2-(4-nitrobenzyl)-[2-(13C)]pyrimidin-5-yl]acetate

Guidance literature:: Multi-step reaction with 4 steps

1.1: tetrabutylammomium bromide / dichloromethane; water / 20 °C

2.1: nitric acid / dichloromethane / 1 h / 0 - 20 °C

3.1: hydrogenchloride / 1,4-dioxane; ethanol / 22 h / 20 °C

3.2: 2.5 h

4.1: sodium methylate / methanol / 1.5 h / Reflux

4.2: 0.5 h / 0 °C

With hydrogenchloride; tetrabutylammomium bromide; nitric acid; sodium methylate; In 1,4-dioxane; methanol; ethanol; dichloromethane; water;

Reference yield:

: 388582-22-7
4-nitrophenylaceto[13C]nitrile

: 1214271-97-2
methyl [4,6-dihydroxy-2-(4-nitrobenzyl)-[2-(13C)]pyrimidin-5-yl]acetate

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydrogenchloride / 1,4-dioxane; ethanol / 22 h / 20 °C

1.2: 2.5 h

2.1: sodium methylate / methanol / 1.5 h / Reflux

2.2: 0.5 h / 0 °C

With hydrogenchloride; sodium methylate; In 1,4-dioxane; methanol; ethanol;