3-Methoxy-4-methoxymethoxy cinnamic acid

Base Information

Chemical Name:3-Methoxy-4-methoxymethoxy cinnamic acid
CAS No.:169959-08-4
Molecular Formula:C₁₂H₁₄O₅
Molecular Weight:238.24
Hs Code.:

Synonyms:3-Methoxy-4-methoxymethoxy cinnamic acid

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Chemical Property of 3-Methoxy-4-methoxymethoxy cinnamic acid

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Technology Process of 3-Methoxy-4-methoxymethoxy cinnamic acid

There total 9 articles about 3-Methoxy-4-methoxymethoxy cinnamic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 1135-24-6,537-98-4
(E)-3-(4-hydroxy-3-methoxyphenyl)acrylic acid

: 107-30-2
chloromethyl methyl ether

: 169959-08-4
3-Methoxy-4-methoxymethoxy cinnamic acid

Guidance literature:: (E)-3-(4-hydroxy-3-methoxyphenyl)acrylic acid; With sodium hydride; In acetonitrile; at 0 ℃; for 0.166667h;

chloromethyl methyl ether; In acetonitrile; for 3h;
DOI:10.1248/cpb.c15-00476

Reference yield:

: 220300-07-2
methyl (E)-4-methoxymethyl-3-methoxycinnamate

: 169959-08-4
3-Methoxy-4-methoxymethoxy cinnamic acid

Guidance literature:: methyl (E)-4-methoxymethyl-3-methoxycinnamate; With water; sodium hydroxide; for 2h;

With acetic acid;
DOI:10.1007/s12039-010-0050-7

Reference yield:

: 121-33-5,8014-42-4
vanillin

: 169959-08-4
3-Methoxy-4-methoxymethoxy cinnamic acid

Guidance literature:: Multi-step reaction with 3 steps

1.1: piperidine; pyridine / 4 h / 100 °C

2.1: potassium carbonate / acetone / 1 h / 20 °C

2.2: 3 h

3.1: sodium hydroxide; water / ethanol / 3 h / Reflux

With piperidine; pyridine; water; potassium carbonate; sodium hydroxide; In ethanol; acetone; 1.1: |Knoevenagel Condensation;
DOI:10.1007/s12039-014-0599-7