Technology Process of C23H33NO7Si
There total 7 articles about C23H33NO7Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
dmap; triethylamine;
In
tetrahydrofuran;
for 12h;
DOI:10.1021/jo010838k
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 79 percent / AcOH / ethanol / 3 h / Heating
2: 72 percent / HCl / acetone / 2 h / 0 °C
3: 88 percent / H2 / 10percent Pd/C / ethanol / 20 °C
4: 86 percent / pyridine / CH2Cl2 / 5 h / 0 °C
5: 90 percent / (CH3)3COK / acetonitrile / 0.5 h / 20 °C
6: 70 percent / imidazole / acetonitrile / 24 h / 20 °C
7: 94 percent / Et3N; DMAP / tetrahydrofuran / 12 h
With
pyridine; 1H-imidazole; hydrogenchloride; dmap; potassium tert-butylate; hydrogen; acetic acid; triethylamine;
10percent Pd/C;
In
tetrahydrofuran; ethanol; dichloromethane; acetone; acetonitrile;
DOI:10.1021/jo010838k
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 72 percent / HCl / acetone / 2 h / 0 °C
2: 88 percent / H2 / 10percent Pd/C / ethanol / 20 °C
3: 86 percent / pyridine / CH2Cl2 / 5 h / 0 °C
4: 90 percent / (CH3)3COK / acetonitrile / 0.5 h / 20 °C
5: 70 percent / imidazole / acetonitrile / 24 h / 20 °C
6: 94 percent / Et3N; DMAP / tetrahydrofuran / 12 h
With
pyridine; 1H-imidazole; hydrogenchloride; dmap; potassium tert-butylate; hydrogen; triethylamine;
10percent Pd/C;
In
tetrahydrofuran; ethanol; dichloromethane; acetone; acetonitrile;
DOI:10.1021/jo010838k
