3-(dibenzo[b,d]thiophen-4-yl)-9-(4,6-diphenyl-1,3,5-triazin-2-yl)-9H-carbazole

Base Information

• Chemical Name: 3-(dibenzo[b,d]thiophen-4-yl)-9-(4,6-diphenyl-1,3,5-triazin-2-yl)-9H-carbazole
• CAS No.: 1346669-09-7
• Molecular Formula: C₃₉H₂₄N₄S
• Molecular Weight: 580.712

Synonyms:3-(dibenzo[b,d]thiophen-4-yl)-9-(4,6-diphenyl-1,3,5-triazin-2-yl)-9H-carbazole

Chemical Property of 3-(dibenzo[b,d]thiophen-4-yl)-9-(4,6-diphenyl-1,3,5-triazin-2-yl)-9H-carbazole

Chemical Property:

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Technology Process of 3-(dibenzo[b,d]thiophen-4-yl)-9-(4,6-diphenyl-1,3,5-triazin-2-yl)-9H-carbazole

There total 7 articles about 3-(dibenzo[b,d]thiophen-4-yl)-9-(4,6-diphenyl-1,3,5-triazin-2-yl)-9H-carbazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.7%

2-chloro-4,6-diphenyl-1,3,5-triazine (3842-55-5) + 3-(dibenzo[b,d]furan-4-yl)-9H-carbazole (1346669-46-2) → 3-(dibenzo[b,d]thiophen-4-yl)-9-(4,6-diphenyl-1,3,5-triazin-2-yl)-9H-carbazole (1346669-09-7)

Guidance literature:

3-(dibenzo[b,d]furan-4-yl)-9H-carbazole; With sodium hydride; In N,N-dimethyl-formamide; for 0.25h; Inert atmosphere;

2-chloro-4,6-diphenyl-1,3,5-triazine; In N,N-dimethyl-formamide; at 20 ℃; Inert atmosphere;

DOI:10.1039/c6ra27770e

Reference yield: 60.0%

4-dibenzothiophene boronic acid (108847-20-7) + 3-bromo-9-(4,6-diphenyl-[1,3,5]triazin-2-yl)-9H-carbazole (1266389-17-6) → 3-(dibenzo[b,d]thiophen-4-yl)-9-(4,6-diphenyl-1,3,5-triazin-2-yl)-9H-carbazole (1346669-09-7)

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In ethanol; toluene; for 12h; Reflux;

Reference yield:

4-bromodibenzothiophene (97511-05-2) + 9-(4,6-diphenyl-1,3,5-triazin-2-yl)-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-9H-carbazole → 3-(dibenzo[b,d]thiophen-4-yl)-9-(4,6-diphenyl-1,3,5-triazin-2-yl)-9H-carbazole (1346669-09-7)

Guidance literature:

With bis(tri-t-butylphosphine)palladium⁽⁰⁾; sodium t-butanolate; In toluene; for 6h; Reflux; Inert atmosphere;

upstream raw materials:

2-chloro-4,6-diphenyl-1,3,5-triazine

9H-carbazole

9-(4,6-diphenyl-1,3,5-triazin-2-yl)-9H-carbazole

4-dibenzothiophene boronic acid

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