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4-BROMODIBENZOTHIOPHENE
Cas No: 97511-05-2
USD $ 600.0-600.0 / Gram 500 Gram 20 Metric Ton/Month Henan Allgreen Chemical Co.,Ltd Contact Supplier
4-Bromodibenzothiophene
Cas No: 97511-05-2
USD $ 3.0-3.0 / Kilogram 1 Kilogram 1-100 Metric Ton/Month Dayang Chem (Hangzhou) Co.,Ltd. Contact Supplier
4-Bromodibenzothiophene
Cas No: 97511-05-2
No Data 10 Milligram Amadis Chemical Co., Ltd. Contact Supplier
High Quality 99% 97511-05-2 4-bromodibenzo[b,d]thiophene Manufacturer
Cas No: 97511-05-2
USD $ 0.1-0.1 / Gram 1 Gram 100 Metric Ton/Year Xi'an Xszo Chem Co., Ltd. Contact Supplier
High purity Made in China 4-Bromodibenzothiophene
Cas No: 97511-05-2
No Data 100 Gram 300 Kilogram/Month Puyang Huicheng Electronic Material Co., Ltd Contact Supplier
4-Bromodibenzothiophene
Cas No: 97511-05-2
USD $ 1.0-1.0 / Kilogram 1 Kilogram 1000 Metric Ton/Year Henan Sinotech Import&Export Corporation Contact Supplier
4-Bromodibenzothiophene
Cas No: 97511-05-2
USD $ 2.0-2.0 / Gram 1 Gram 100 Metric Ton/Year Jinan Finer Chemical Co., Ltd Contact Supplier
best offer 4-BROMODIBENZOTHIOPHENE
Cas No: 97511-05-2
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Factory direct supply CAS 97511-05-2 with best quality
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USD $ 139.0-210.0 / Kilogram 1 Kilogram 1000 Kilogram/Day Zhuozhou Wenxi import and Export Co., Ltd Contact Supplier
BLOOM TECH Advanced API/Technology support 4-Bromodibenzo[b,d]thiophene CAS 97511-05-2
Cas No: 97511-05-2
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97511-05-2 Usage

97511-05-2SDS

SAFETY DATA SHEETS

According to Globally Harmonized System of Classification and Labelling of Chemicals (GHS) - Sixth revised edition

Version: 1.0

Creation Date: Aug 12, 2017

Revision Date: Aug 12, 2017

1.Identification

1.1 GHS Product identifier

Product name 4-Bromodibenzothiophene

1.2 Other means of identification

Product number -
Other names 4-BROMODIBENZOTHIOPHENE

1.3 Recommended use of the chemical and restrictions on use

Identified uses For industry use only.
Uses advised against no data available

1.4 Supplier's details

1.5 Emergency phone number

Emergency phone number -
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More Details:97511-05-2 SDS

97511-05-2Synthetic route

dibenzothiophene
132-65-0

dibenzothiophene

4-bromodibenzothiophene
97511-05-2

4-bromodibenzothiophene

Conditions
ConditionsYield
Stage #1: dibenzothiophene With n-butyllithium In tetrahydrofuran at -40 - 0℃; for 7h;
Stage #2: With ethylene dibromide In tetrahydrofuran at -78 - 20℃; for 12h;
95%
Stage #1: dibenzothiophene With n-butyllithium In tetrahydrofuran at -40 - 0℃; for 6h;
Stage #2: With ethylene dibromide In tetrahydrofuran at -78 - 20℃; for 14h;
71%
Stage #1: dibenzothiophene With n-butyllithium In tetrahydrofuran at -78 - 0℃;
Stage #2: With ethylene dibromide In tetrahydrofuran at -78 - 20℃; for 12h;
60%
3-bromo-2-(methylsulfinyl)-1,1‘-biphenyl

3-bromo-2-(methylsulfinyl)-1,1‘-biphenyl

4-bromodibenzothiophene
97511-05-2

4-bromodibenzothiophene

Conditions
ConditionsYield
Stage #1: 3-bromo-2-(methylsulfinyl)-1,1‘-biphenyl With trifluoroacetic acid at 20℃; for 24h;
Stage #2: With pyridine In water for 0.5h; Reflux;
88%
Stage #1: 3-bromo-2-(methylsulfinyl)-1,1‘-biphenyl With trifluorormethanesulfonic acid at 20℃; for 24h;
Stage #2: With pyridine In water for 0.5h; Reflux;
81%
Stage #1: 3-bromo-2-(methylsulfinyl)-1,1‘-biphenyl With trifluorormethanesulfonic acid In water at 20℃; for 24h;
Stage #2: With pyridine In water for 0.5h; Reflux;
81%
4-bromo-dibenzo[b,d]thiophene S-oxide

4-bromo-dibenzo[b,d]thiophene S-oxide

A

dibenzothiophene
132-65-0

dibenzothiophene

B

Dibenzothiophene sulfoxide
1013-23-6

Dibenzothiophene sulfoxide

C

4-bromodibenzothiophene
97511-05-2

4-bromodibenzothiophene

Conditions
ConditionsYield
In acetonitrile Quantum yield; Photolysis;
biphenyl
92-52-4

biphenyl

4-bromodibenzothiophene
97511-05-2

4-bromodibenzothiophene

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: aluminium chloride; sulfur
2: butyl lithium; diethyl ether / Behandeln der Reaktionsloesung mit Brom-Dampf in Stickstoff-Strom
View Scheme
4-bromodibenzothiophene
97511-05-2

4-bromodibenzothiophene

4-bromo-dibenzo[b,d]thiophene S-oxide

4-bromo-dibenzo[b,d]thiophene S-oxide

Conditions
ConditionsYield
With boron trifluoride diethyl etherate; 3-chloro-benzenecarboperoxoic acid In hexane; dichloromethane at -30℃; Inert atmosphere;99%
With 3-chloro-benzenecarboperoxoic acid In dichloromethane at -30℃; for 1.5h;50%
With 3-chloro-benzenecarboperoxoic acid In dichloromethane at 0℃; for 2h; Inert atmosphere;
4-bromodibenzothiophene
97511-05-2

4-bromodibenzothiophene

(2-methylsulfanylphenyl)boronic acid
168618-42-6

(2-methylsulfanylphenyl)boronic acid

4-[2-(methylthio)phenyl]dibenzothiophene

4-[2-(methylthio)phenyl]dibenzothiophene

Conditions
ConditionsYield
With tetrakis(triphenylphosphine) palladium(0); sodium carbonate In ethanol; water; toluene at 120℃; for 3h; Suzuki Coupling;99%
4-bromodibenzothiophene
97511-05-2

4-bromodibenzothiophene

(2’-fluoro-[1,1’-biphenyl]2-yl)boronic acid

(2’-fluoro-[1,1’-biphenyl]2-yl)boronic acid

4-(2'-fluoro-[1,1'-biphenyl]-2-yl)dibenzo[b,d]thiophene

4-(2'-fluoro-[1,1'-biphenyl]-2-yl)dibenzo[b,d]thiophene

Conditions
ConditionsYield
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In methanol; water; toluene for 18h; Suzuki Coupling; Inert atmosphere; Reflux;99%
4-bromodibenzothiophene
97511-05-2

4-bromodibenzothiophene

phenylboronic acid
98-80-6

phenylboronic acid

4-phenyldibenzo[b,d]thiophene
98251-31-1

4-phenyldibenzo[b,d]thiophene

Conditions
ConditionsYield
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In 1,2-dimethoxyethane; water at 80℃; for 24h; Inert atmosphere;97%
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In ethanol; water; toluene at 100℃; for 18h; Inert atmosphere;84%
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In ethanol; water; toluene Reflux;82%
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In ethanol; water; toluene Reflux;82%
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In ethanol; water; toluene at 80℃; for 3.5h;
4-bromodibenzothiophene
97511-05-2

4-bromodibenzothiophene

bis(pinacol)diborane
73183-34-3

bis(pinacol)diborane

2-(dibenzo[b,d]thiophen-4-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
912824-84-1

2-(dibenzo[b,d]thiophen-4-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Conditions
ConditionsYield
With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate In 1,4-dioxane Reflux;95%
With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate In N,N-dimethyl-formamide at 90℃;90%
With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate In N,N-dimethyl-formamide at 120℃;80%
4-bromodibenzothiophene
97511-05-2

4-bromodibenzothiophene

C39H33BN4O2

C39H33BN4O2

C45H28N4S

C45H28N4S

Conditions
ConditionsYield
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In tetrahydrofuran; water at 80℃; for 12h; Inert atmosphere;95%
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In tetrahydrofuran; water at 80℃; for 12h; Inert atmosphere;92%
tetrahydrofuran
109-99-9

tetrahydrofuran

4-bromodibenzothiophene
97511-05-2

4-bromodibenzothiophene

2-(dibenzo[b,d]thiophen-4-yl)tetrahydrofuran

2-(dibenzo[b,d]thiophen-4-yl)tetrahydrofuran

Conditions
ConditionsYield
With bis(acetylacetonate)nickel(II); 5,5'-dimethyl-2,2'-bipyridine; (4-methoxyphenyl)(4-(trifluoromethyl)phenyl)methanone; sodium carbonate at 20℃; for 60h; Schlenk technique; Inert atmosphere; Irradiation; chemoselective reaction;93%
4-bromodibenzothiophene
97511-05-2

4-bromodibenzothiophene

C12H7BrO2S

C12H7BrO2S

Conditions
ConditionsYield
With dihydrogen peroxide; acetic acid In tetrahydrofuran at 80℃; for 2h;93%
4-bromodibenzothiophene
97511-05-2

4-bromodibenzothiophene

aniline
62-53-3

aniline

N-(dibenzothiophene-4-yl)-N-phenyl-amine
1252914-52-5

N-(dibenzothiophene-4-yl)-N-phenyl-amine

Conditions
ConditionsYield
Stage #1: 4-bromodibenzothiophene; aniline With sodium t-butanolate In toluene for 1h; Inert atmosphere;
Stage #2: With tris-(dibenzylideneacetone)dipalladium(0); tri tert-butylphosphoniumtetrafluoroborate In toluene for 2h; Inert atmosphere; Reflux;
91%
With tri-tert-butyl phosphine; potassium tert-butylate; palladium diacetate In toluene at 100℃; for 10h; Inert atmosphere; Schlenk technique; Sealed tube;86%
With tri-tert-butyl phosphine; potassium tert-butylate; palladium diacetate In toluene at 100℃; for 7h; Schlenk technique; Inert atmosphere;77.8%
4-bromodibenzothiophene
97511-05-2

4-bromodibenzothiophene

2-carbomethoxyaniline
134-20-3

2-carbomethoxyaniline

methyl 2-(dibenzo[b,d]thiophen-4-ylamino)benzoate

methyl 2-(dibenzo[b,d]thiophen-4-ylamino)benzoate

Conditions
ConditionsYield
With palladium diacetate; caesium carbonate; bis[2-(diphenylphosphino)phenyl] ether In toluene at 110℃; Inert atmosphere;90%
Stage #1: 4-bromodibenzothiophene With palladium diacetate; caesium carbonate; 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene for 3h;
Stage #2: 2-carbomethoxyaniline In toluene Reflux;
86.8%
With palladium diacetate; caesium carbonate; 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene for 24h; Buchwald-Hartwig Coupling; Reflux; Inert atmosphere;
4-bromodibenzothiophene
97511-05-2

4-bromodibenzothiophene

(6-phenyldibenzo[b,d]furan-4-yl)boronic acid
1010068-85-5

(6-phenyldibenzo[b,d]furan-4-yl)boronic acid

C30H18OS

C30H18OS

Conditions
ConditionsYield
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In ethanol; water; toluene Reflux;89%
4-bromodibenzothiophene
97511-05-2

4-bromodibenzothiophene

2-methoxycarbonylphenylboronic acid
374538-03-1

2-methoxycarbonylphenylboronic acid

C20H14O2S

C20H14O2S

Conditions
ConditionsYield
With tetrakis(triphenylphosphine) palladium(0); sodium carbonate In ethanol; water; toluene at 95 - 100℃; Inert atmosphere;87.4%
4-bromodibenzothiophene
97511-05-2

4-bromodibenzothiophene

4-hydroxydibenzothiophene
24444-75-5

4-hydroxydibenzothiophene

Conditions
ConditionsYield
With tris-(dibenzylideneacetone)dipalladium(0); potassium hydroxide; tert-butyl XPhos In 1,4-dioxane; water at 100℃; for 16h;87%
With sodium hydroxide; copper In water at 240 - 260℃; for 24h; autoclave;72%
4-bromodibenzothiophene
97511-05-2

4-bromodibenzothiophene

C32H21NS

C32H21NS

C44H27NS2

C44H27NS2

Conditions
ConditionsYield
With tri-tert-butyl phosphine; bis(dibenzylideneacetone)-palladium(0); sodium t-butanolate In toluene Inert atmosphere; Reflux;87%
4-bromodibenzothiophene
97511-05-2

4-bromodibenzothiophene

(6-phenyldibenzo[b,d]thiophen-4-yl)boronic acid
1115640-18-0

(6-phenyldibenzo[b,d]thiophen-4-yl)boronic acid

C30H18S2

C30H18S2

Conditions
ConditionsYield
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In ethanol; water; toluene Reflux;86%
4-bromodibenzothiophene
97511-05-2

4-bromodibenzothiophene

C36H21NS4

C36H21NS4

C48H27NS5

C48H27NS5

Conditions
ConditionsYield
With copper; potassium carbonate In nitrobenzene for 16h; Inert atmosphere; Reflux;85%
4-bromodibenzothiophene
97511-05-2

4-bromodibenzothiophene

para-thiocresol
106-45-6

para-thiocresol

4-(p-tolylthio)dibenzo[b,d]thiophene
113525-43-2

4-(p-tolylthio)dibenzo[b,d]thiophene

Conditions
ConditionsYield
With nickel(II) bromide dimethoxyethane; 4,4'-di-tert-butyl-2,2'-bipyridine; lithium bromide In N,N-dimethyl-formamide at 20℃; for 6h; Electrochemical reaction;85%
4-bromodibenzothiophene
97511-05-2

4-bromodibenzothiophene

3-chloro-6-(dibenzo[b,d]furan-4-yl)-9H-carbazole

3-chloro-6-(dibenzo[b,d]furan-4-yl)-9H-carbazole

3-chloro-6-(dibenzo[b,d]furan-4-yl)-9-(dibenzo[b,d]thiophen-4-yl)-9H-carbazole

3-chloro-6-(dibenzo[b,d]furan-4-yl)-9-(dibenzo[b,d]thiophen-4-yl)-9H-carbazole

Conditions
ConditionsYield
With tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine; sodium t-butanolate In toluene at 110℃; for 4h;85%
4-bromodibenzothiophene
97511-05-2

4-bromodibenzothiophene

zinc(II) chloride
7646-85-7

zinc(II) chloride

C12H7BrSZn

C12H7BrSZn

Conditions
ConditionsYield
With magnesium; fullerene-C60; lithium chloride In tetrahydrofuran; 1,2-dimethoxyethane at 25℃; for 1h; Schlenk technique; Inert atmosphere;84%
4-bromodibenzothiophene
97511-05-2

4-bromodibenzothiophene

C36H23NOS

C36H23NOS

C48H29NOS2

C48H29NOS2

Conditions
ConditionsYield
With tri-tert-butyl phosphine; bis(dibenzylideneacetone)-palladium(0); sodium t-butanolate In toluene Reflux; Inert atmosphere;84%
4-bromodibenzothiophene
97511-05-2

4-bromodibenzothiophene

2-(carbazol-9-yl)-9H-carbazole
1226810-15-6

2-(carbazol-9-yl)-9H-carbazole

9-(dibenzo[b,d]thiophen-4-yl)-9H-2,9'-bicarbazole

9-(dibenzo[b,d]thiophen-4-yl)-9H-2,9'-bicarbazole

Conditions
ConditionsYield
With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; tris-(dibenzylideneacetone)dipalladium(0); sodium t-butanolate In 5,5-dimethyl-1,3-cyclohexadiene for 24h; Reflux; Inert atmosphere;83%
4-bromodibenzothiophene
97511-05-2

4-bromodibenzothiophene

dibenzo[b,d]thiophene-4-carboxamide
197571-97-4

dibenzo[b,d]thiophene-4-carboxamide

Conditions
ConditionsYield
With 1H-imidazole; 1,1'-bis-(diphenylphosphino)ferrocene; palladium diacetate; ammonium chloride; N-ethyl-N,N-diisopropylamine In 1,4-dioxane at 90℃; for 3h; Sealed tube;82%
4-bromodibenzothiophene
97511-05-2

4-bromodibenzothiophene

Trimethyl borate
121-43-7

Trimethyl borate

4-dibenzothiophene boronic acid
108847-20-7

4-dibenzothiophene boronic acid

Conditions
ConditionsYield
Stage #1: 4-bromodibenzothiophene With n-butyllithium In tetrahydrofuran at -78 - 0℃; for 1h;
Stage #2: Trimethyl borate In tetrahydrofuran at -78 - 20℃; for 12h;
82%
Stage #1: 4-bromodibenzothiophene With n-butyllithium In tetrahydrofuran for 2h; Cooling with acetone-dry ice;
Stage #2: Trimethyl borate In tetrahydrofuran at -78 - 0℃; for 1h;
Stage #3: With hydrogenchloride In tetrahydrofuran; water at 0 - 20℃; for 8h;
Stage #1: 4-bromodibenzothiophene With n-butyllithium at -78 - 0℃;
Stage #2: Trimethyl borate at -78 - 20℃;
Stage #3: With hydrogenchloride In water at 0 - 20℃;
4-bromodibenzothiophene
97511-05-2

4-bromodibenzothiophene

C18H13NS2

C18H13NS2

C30H19NS3

C30H19NS3

Conditions
ConditionsYield
With tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine; sodium t-butanolate In toluene for 6h; Inert atmosphere; Reflux;81%
4-bromodibenzothiophene
97511-05-2

4-bromodibenzothiophene

4-(phenanthren-9-yl)aniline

4-(phenanthren-9-yl)aniline

C32H21NS

C32H21NS

Conditions
ConditionsYield
With tri-tert-butyl phosphine; bis(dibenzylideneacetone)-palladium(0); sodium t-butanolate In toluene Reflux; Inert atmosphere;81%
4-bromodibenzothiophene
97511-05-2

4-bromodibenzothiophene

9-(9H-carbazol-3-yl)-9H-carbazole
18628-07-4

9-(9H-carbazol-3-yl)-9H-carbazole

9-(dibenzo[b,d]thiophen-4-yl)-9H-3,9'-bicarbazole

9-(dibenzo[b,d]thiophen-4-yl)-9H-3,9'-bicarbazole

Conditions
ConditionsYield
With copper(l) iodide; XPhos In 5,5-dimethyl-1,3-cyclohexadiene for 216h; Inert atmosphere; Reflux;81%
With potassium phosphate; copper(l) iodide; rac-diaminocyclohexane In 5,5-dimethyl-1,3-cyclohexadiene for 576h; Inert atmosphere; Reflux;81%
4-bromodibenzothiophene
97511-05-2

4-bromodibenzothiophene

C45H36BN3O2

C45H36BN3O2

C51H31N3S

C51H31N3S

Conditions
ConditionsYield
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In ethanol; water; toluene Reflux;80%
4-bromodibenzothiophene
97511-05-2

4-bromodibenzothiophene

3-chloro-6-(dibenzo[b,d]furan-3-yl)-9H-carbazole

3-chloro-6-(dibenzo[b,d]furan-3-yl)-9H-carbazole

3-chloro-6-(dibenzo[b,d]furan-3-yl)-9-(dibenzo[b,d]thiophen-4-yl)-9H-carbazole

3-chloro-6-(dibenzo[b,d]furan-3-yl)-9-(dibenzo[b,d]thiophen-4-yl)-9H-carbazole

Conditions
ConditionsYield
With tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine; sodium t-butanolate In toluene at 110℃; for 4h;80%
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