methyl 5-amino-3-(1,1-dioxidotetrahydro-2H-1,2-thiazin-2-yl)-2-fluorobenzoate

Base Information

Chemical Name:methyl 5-amino-3-(1,1-dioxidotetrahydro-2H-1,2-thiazin-2-yl)-2-fluorobenzoate
CAS No.:706792-66-7
Molecular Formula:C₁₂H₁₅FN₂O₄S
Molecular Weight:302.327
Hs Code.:

Synonyms:methyl 5-amino-3-(1,1-dioxidotetrahydro-2H-1,2-thiazin-2-yl)-2-fluorobenzoate

Suppliers and Price of methyl 5-amino-3-(1,1-dioxidotetrahydro-2H-1,2-thiazin-2-yl)-2-fluorobenzoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of methyl 5-amino-3-(1,1-dioxidotetrahydro-2H-1,2-thiazin-2-yl)-2-fluorobenzoate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of methyl 5-amino-3-(1,1-dioxidotetrahydro-2H-1,2-thiazin-2-yl)-2-fluorobenzoate

There total 5 articles about methyl 5-amino-3-(1,1-dioxidotetrahydro-2H-1,2-thiazin-2-yl)-2-fluorobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 706792-62-3
methyl 3-(1,1-dioxidotetrahydro-2H-1,2-thiazin-2-yl)-2-fluoro-5-nitrobenzoate

: 706792-66-7
methyl 5-amino-3-(1,1-dioxidotetrahydro-2H-1,2-thiazin-2-yl)-2-fluorobenzoate

Guidance literature:: With aq. NH₄CO₂H; palladium on activated charcoal; In ethanol; Heating;
DOI:10.1016/j.bmcl.2007.12.020

Reference yield:

: 706818-91-9
methyl 3-amino-2-fluoro-5-nitrobenzoate

: 706792-66-7
methyl 5-amino-3-(1,1-dioxidotetrahydro-2H-1,2-thiazin-2-yl)-2-fluorobenzoate

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / dichloromethane / 0 - 20 °C

2: triethylamine / methanol / 2 h / Heating / reflux

3: iron; acetic acid / water / 2 h / 50 °C

With iron; acetic acid; triethylamine; In methanol; dichloromethane; water;

Reference yield:

: 367946-80-3
methyl 2-fluoro-3,5-dinitrobenzoic ester

: 706792-66-7
methyl 5-amino-3-(1,1-dioxidotetrahydro-2H-1,2-thiazin-2-yl)-2-fluorobenzoate

Guidance literature:: Multi-step reaction with 4 steps

1: iron; acetic acid / water / 3 h / 20 - 35 °C

2: triethylamine / dichloromethane / 0 - 20 °C

3: triethylamine / methanol / 2 h / Heating / reflux

4: iron; acetic acid / water / 2 h / 50 °C

With iron; acetic acid; triethylamine; In methanol; dichloromethane; water;