Dimethyl 5-hydroxy-3-methoxy-4-methylphthalate

Base Information Edit

Chemical Name:Dimethyl 5-hydroxy-3-methoxy-4-methylphthalate
CAS No.:219646-64-7
Molecular Formula:C₁₂H₁₄O₆
Molecular Weight:254.24
Hs Code.:
DSSTox Substance ID:DTXSID201334436
Mol file:219646-64-7.mol

Synonyms:dimethyl 5-hydroxy-3-methoxy-4-methylphthalate;219646-64-7;DTXSID201334436

Suppliers and Price of Dimethyl 5-hydroxy-3-methoxy-4-methylphthalate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Dimethyl 5-hydroxy-3-methoxy-4-methylphthalate Edit

Chemical Property:

XLogP3:1.6
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:5
Exact Mass:254.07903816
Heavy Atom Count:18
Complexity:316

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1=C(C=C(C(=C1OC)C(=O)OC)C(=O)OC)O

Technology Process of Dimethyl 5-hydroxy-3-methoxy-4-methylphthalate

There total 2 articles about Dimethyl 5-hydroxy-3-methoxy-4-methylphthalate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 219646-62-5
TMSOC₆H₅MeOMe

: 762-42-5
dimethyl acetylenedicarboxylate

: 219646-64-7
dimethyl 5-hydroxy-3-methoxy-4-methylphthalate

Guidance literature:: TMSOC₆H₅MeOMe; dimethyl acetylenedicarboxylate; In 5,5-dimethyl-1,3-cyclohexadiene; at -10 ℃; for 2h;

at 120 ℃; for 2h;
DOI:10.1055/s-0033-1340060

Reference yield:

: 25112-91-8
3-methoxy-2-methylcyclohex-2-en-1-one

: 762-42-5
dimethyl acetylenedicarboxylate

: 219646-64-7
dimethyl 5-hydroxy-3-methoxy-4-methylphthalate

Guidance literature:: With chloro-trimethyl-silane; lithium diisopropyl amide; Yield given; Multistep reaction; 1) THF, -70 deg C, 65 min; 2) xylene, rt, 2 h, 70 deg c, 2 h, 120 deg C, 3 h;