CH₃C(C₆H₅)N((CH₃)2C₆H₃)C₃H₃N₂⁽¹⁺⁾*Cl^(1-)=CH₃C(C₆H₅)N((CH₃)2C₆H₃)C₃H₃N₂Cl

Base Information

Chemical Name:CH₃C(C₆H₅)N((CH₃)2C₆H₃)C₃H₃N₂⁽¹⁺⁾*Cl^(1-)=CH₃C(C₆H₅)N((CH₃)2C₆H₃)C₃H₃N₂Cl
CAS No.:1095281-87-0
Molecular Formula:C₁₉H₂₀N₃*Cl
Molecular Weight:325.841
Hs Code.:

CH<sub>3</sub>C(C<sub>6</sub>H<sub>5</sub>)N((CH<sub>3</sub>)2C<sub>6</sub>H<sub>3</sub>)C<sub>3</sub>H<sub>3</sub>N<sub>2</sub><sup>(1+)</sup>*Cl<sup>(1-)</sup>=CH<sub>3</sub>C(C<sub>6</sub>H<sub>5</sub>)N((CH<sub>3</sub>)2C<sub>6</sub>H<sub>3</sub>)C<sub>3</sub>H<sub>3</sub>N<sub>2</sub>Cl

Synonyms:CH₃C(C₆H₅)N((CH₃)2C₆H₃)C₃H₃N₂⁽¹⁺⁾*Cl^(1-)=CH₃C(C₆H₅)N((CH₃)2C₆H₃)C₃H₃N₂Cl

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Chemical Property of CH₃C(C₆H₅)N((CH₃)2C₆H₃)C₃H₃N₂⁽¹⁺⁾*Cl^(1-)=CH₃C(C₆H₅)N((CH₃)2C₆H₃)C₃H₃N₂Cl

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Technology Process of CH₃C(C₆H₅)N((CH₃)2C₆H₃)C₃H₃N₂⁽¹⁺⁾*Cl^(1-)=CH₃C(C₆H₅)N((CH₃)2C₆H₃)C₃H₃N₂Cl

There total 4 articles about CH₃C(C₆H₅)N((CH₃)2C₆H₃)C₃H₃N₂⁽¹⁺⁾*Cl^(1-)=CH₃C(C₆H₅)N((CH₃)2C₆H₃)C₃H₃N₂Cl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 616-47-7
1-methyl-1H-imidazole

: 59387-01-8
N-(2,6-dimethylphenyl)benzenecarboximidoyl chloride

: 1095281-87-0
CH₃C(C₆H₅)N((CH₃)2C₆H₃)C₃H₃N₂⁽¹⁺⁾*Cl^(1-)=CH₃C(C₆H₅)N((CH₃)2C₆H₃)C₃H₃N₂Cl

Guidance literature:: In tetrahydrofuran; at 20 ℃; for 67h;
DOI:10.1016/j.jorganchem.2008.09.006

Reference yield:

: 98-88-4
benzoyl chloride

: 1095281-87-0
CH₃C(C₆H₅)N((CH₃)2C₆H₃)C₃H₃N₂⁽¹⁺⁾*Cl^(1-)=CH₃C(C₆H₅)N((CH₃)2C₆H₃)C₃H₃N₂Cl

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / dichloromethane / 48 h / Reflux

2: thionyl chloride / 3 h / Reflux

3: tetrahydrofuran / 96 h / 20 °C

With thionyl chloride; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1039/c1nj20343f

Reference yield:

: 18109-39-2
N-(2,6-diimethylphenyl)benzamide

: 1095281-87-0
CH₃C(C₆H₅)N((CH₃)2C₆H₃)C₃H₃N₂⁽¹⁺⁾*Cl^(1-)=CH₃C(C₆H₅)N((CH₃)2C₆H₃)C₃H₃N₂Cl

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride / 3 h / Reflux

2: tetrahydrofuran / 96 h / 20 °C

With thionyl chloride; In tetrahydrofuran;
DOI:10.1039/c1nj20343f