ethyl 1-((tert-butyldimethylsilyloxy)methyl)-2-oxocyclohexanecarboxylate

Base Information

Chemical Name:ethyl 1-((tert-butyldimethylsilyloxy)methyl)-2-oxocyclohexanecarboxylate
CAS No.:1138530-46-7
Molecular Formula:C₁₆H₃₀O₄Si
Molecular Weight:314.497
Hs Code.:

Synonyms:ethyl 1-((tert-butyldimethylsilyloxy)methyl)-2-oxocyclohexanecarboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethyl 1-((tert-butyldimethylsilyloxy)methyl)-2-oxocyclohexanecarboxylate

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Technology Process of ethyl 1-((tert-butyldimethylsilyloxy)methyl)-2-oxocyclohexanecarboxylate

There total 1 articles about ethyl 1-((tert-butyldimethylsilyloxy)methyl)-2-oxocyclohexanecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 133295-89-3
ethyl 1-(hydroxymethyl)-2-oxocyclohexanecarboxylate

: 18162-48-6
tert-butyldimethylsilyl chloride

: 1138530-46-7
ethyl 1-((tert-butyldimethylsilyloxy)methyl)-2-oxocyclohexanecarboxylate

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; at 20 ℃; for 16h; Inert atmosphere;
DOI:10.1021/jo900088x

Reference yield: 87.0%

: 1138530-46-7
ethyl 1-((tert-butyldimethylsilyloxy)methyl)-2-oxocyclohexanecarboxylate

: 1779-49-3
Methyltriphenylphosphonium bromide

: 1138529-99-3
ethyl 1-((tert-butyldimethylsilyloxy)methyl)-2-methylenecyclohexanecarboxylate

Guidance literature:: Methyltriphenylphosphonium bromide; With n-butyllithium; In diethyl ether; hexane; at 20 ℃; for 0.5h; Inert atmosphere;

ethyl 1-((tert-butyldimethylsilyloxy)methyl)-2-oxocyclohexanecarboxylate; In diethyl ether; hexane; at 20 ℃; Inert atmosphere; Reflux;
DOI:10.1021/jo900088x