RAC-N-BENZYL-N-[2-HYDROXYL-2-(4-BENZYLOXY-3-AMINOPHENYL)-ETHYL]-3-(4-METHOXYPHENYL)-2-PROPYLAMINE-D6

Base Information

• Chemical Name: RAC-N-BENZYL-N-[2-HYDROXYL-2-(4-BENZYLOXY-3-AMINOPHENYL)-ETHYL]-3-(4-METHOXYPHENYL)-2-PROPYLAMINE-D6
• CAS No.: 43229-68-1
• Molecular Formula: C₃₂H₃₆N₂O₃
• Molecular Weight: 496.649
• Mol file: 43229-68-1.mol

Synonyms:1-(4-benzyloxy-3-aminobenzene)-2-{benzyl-[2-(4-methoxyphenyl)-1-methylethyl]amino}ethanol

Chemical Property of RAC-N-BENZYL-N-[2-HYDROXYL-2-(4-BENZYLOXY-3-AMINOPHENYL)-ETHYL]-3-(4-METHOXYPHENYL)-2-PROPYLAMINE-D6

Chemical Property:

• Melting Point: >75°C (dec.)
• Storage Temp.: Hygroscopic, -20°C Freezer, Under inert atmosphere
• Solubility.: Chloroform, Dimethylformamide, Dimethyl Sulfoxide, Ethyl Acetate

Purity/Quality:

99% ^*data from raw suppliers

3-Amino-α-[[[2-(4-methoxyphenyl)-1-methylethyl](phenylmethyl)amino]methyl]-4-(phenylmethoxy)benzenemethanol ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Uses: 3-Amino-α-[[[2-(4-methoxyphenyl)-1-methylethyl](phenylmethyl)amino]methyl]-4-(phenylmethoxy)benzenemethanol is an intermediate in the synthesis of Formoterol Fumarate (F693401).

Technology Process of RAC-N-BENZYL-N-[2-HYDROXYL-2-(4-BENZYLOXY-3-AMINOPHENYL)-ETHYL]-3-(4-METHOXYPHENYL)-2-PROPYLAMINE-D6

There total 4 articles about RAC-N-BENZYL-N-[2-HYDROXYL-2-(4-BENZYLOXY-3-AMINOPHENYL)-ETHYL]-3-(4-METHOXYPHENYL)-2-PROPYLAMINE-D6 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.43%

C32H36N2O3*C4H4O4 → 1-(4-benzyloxy-3-aminobenzene)-2-{benzyl-[2-(4-methoxyphenyl)-1-methylethyl]amino}ethanol (43229-68-1)

Guidance literature:

With sodium carbonate; In dichloromethane; water; at 30 - 40 ℃; Temperature;

Reference yield:

1-(4-benzyloxy-3-nitrobenzene)-2-{benzyl-[2-(4-methoxyphenyl)-1-methylethyl]amino}ethanol (43229-67-0) → 1-(4-benzyloxy-3-aminobenzene)-2-{benzyl-[2-(4-methoxyphenyl)-1-methylethyl]amino}ethanol (43229-68-1)

Guidance literature:

With iron; ammonium chloride; In ethanol; water; at 75 - 85 ℃;

Reference yield:

[2-(4-methoxyphenyl)-1-methylethyl](phenylmethyl)amine (43229-65-8) → 1-(4-benzyloxy-3-aminobenzene)-2-{benzyl-[2-(4-methoxyphenyl)-1-methylethyl]amino}ethanol (43229-68-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 90 - 130 °C

2: iron; ammonium chloride / ethanol; water / 75 - 85 °C

With iron; ammonium chloride; In ethanol; water;

upstream raw materials:

[2-(4-methoxyphenyl)-1-methylethyl](phenylmethyl)amine

1-(4-benzyloxy-3-nitrobenzene)-2-{benzyl-[2-(4-methoxyphenyl)-1-methylethyl]amino}ethanol

Downstream raw materials:

N-[5-(2-{Benzyl-[2-(4-methoxy-phenyl)-1-methyl-ethyl]-amino}-1-hydroxy-ethyl)-2-benzyloxy-phenyl]-formamide; compound with (E)-but-2-enedioic acid

formoterol fumarate

formoterol

N-[5-(2-{benzyl[2-(4-methoxyphenyl)-1-methylethyl]amino}-1-hydroxyethyl)-2-benzyloxyphenyl]formamide

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