N-[5-(2-{Benzyl-[2-(4-methoxy-phenyl)-1-methyl-ethyl]-amino}-1-hydroxy-ethyl)-2-benzyloxy-phenyl]-formamide; compound with (E)-but-2-enedioic acid

Base Information

Chemical Name:N-[5-(2-{Benzyl-[2-(4-methoxy-phenyl)-1-methyl-ethyl]-amino}-1-hydroxy-ethyl)-2-benzyloxy-phenyl]-formamide; compound with (E)-but-2-enedioic acid
CAS No.:43229-69-2
Molecular Formula:C₄H₄O₄*C₃₃H₃₆N₂O₄
Molecular Weight:640.733
Hs Code.:

Synonyms:N-[5-(2-{Benzyl-[2-(4-methoxy-phenyl)-1-methyl-ethyl]-amino}-1-hydroxy-ethyl)-2-benzyloxy-phenyl]-formamide; compound with (E)-but-2-enedioic acid

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Chemical Property of N-[5-(2-{Benzyl-[2-(4-methoxy-phenyl)-1-methyl-ethyl]-amino}-1-hydroxy-ethyl)-2-benzyloxy-phenyl]-formamide; compound with (E)-but-2-enedioic acid

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Technology Process of N-[5-(2-{Benzyl-[2-(4-methoxy-phenyl)-1-methyl-ethyl]-amino}-1-hydroxy-ethyl)-2-benzyloxy-phenyl]-formamide; compound with (E)-but-2-enedioic acid

There total 6 articles about N-[5-(2-{Benzyl-[2-(4-methoxy-phenyl)-1-methyl-ethyl]-amino}-1-hydroxy-ethyl)-2-benzyloxy-phenyl]-formamide; compound with (E)-but-2-enedioic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.42%

: 64-18-6
formic acid

: 43229-68-1
1-(4-benzyloxy-3-aminobenzene)-2-{benzyl-[2-(4-methoxyphenyl)-1-methylethyl]amino}ethanol

: 43229-69-2
N-[5-(2-{Benzyl-[2-(4-methoxy-phenyl)-1-methyl-ethyl]-amino}-1-hydroxy-ethyl)-2-benzyloxy-phenyl]-formamide; compound with (E)-but-2-enedioic acid

Guidance literature:: With HATU; In chloroform; at 0 - 10 ℃; Reagent/catalyst; Solvent; Inert atmosphere;

Reference yield:

: 43229-69-2,64196-08-3,143687-24-5,143687-26-7
N-[5-((R)-2-{Benzyl-[2-(4-methoxy-phenyl)-1-methyl-ethyl]-amino}-1-hydroxy-ethyl)-2-benzyloxy-phenyl]-formamide; compound with (E)-but-2-enedioic acid

Guidance literature:: Isomerengemisch VIn, Fumarsaeure;

Reference yield:

: 43229-67-0
1-(4-benzyloxy-3-nitrobenzene)-2-{benzyl-[2-(4-methoxyphenyl)-1-methylethyl]amino}ethanol

: 43229-69-2
N-[5-(2-{Benzyl-[2-(4-methoxy-phenyl)-1-methyl-ethyl]-amino}-1-hydroxy-ethyl)-2-benzyloxy-phenyl]-formamide; compound with (E)-but-2-enedioic acid

Guidance literature:: Multi-step reaction with 2 steps

1: iron; ammonium chloride / ethanol; water / 75 - 85 °C

2: HATU / chloroform / 0 - 10 °C / Inert atmosphere

With iron; ammonium chloride; HATU; In ethanol; chloroform; water;