2,2-bis(benzyloxymethyl)-3-fluoro-1-(((2-nitrophenyl)selenyl)methyl)cyclopropane

Base Information

Chemical Name:2,2-bis(benzyloxymethyl)-3-fluoro-1-(((2-nitrophenyl)selenyl)methyl)cyclopropane
CAS No.:1012785-62-4
Molecular Formula:C₂₆H₂₆FNO₄Se
Molecular Weight:514.455
Hs Code.:

Synonyms:2,2-bis(benzyloxymethyl)-3-fluoro-1-(((2-nitrophenyl)selenyl)methyl)cyclopropane

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Chemical Property of 2,2-bis(benzyloxymethyl)-3-fluoro-1-(((2-nitrophenyl)selenyl)methyl)cyclopropane

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Technology Process of 2,2-bis(benzyloxymethyl)-3-fluoro-1-(((2-nitrophenyl)selenyl)methyl)cyclopropane

There total 4 articles about 2,2-bis(benzyloxymethyl)-3-fluoro-1-(((2-nitrophenyl)selenyl)methyl)cyclopropane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: (2-nitrophenyl)seleno cyanate

: 604785-90-2
2,2-bis(benzyloxymethyl)-3-fluoro-1-(hydroxymethyl)cyclopropane

: 1012785-62-4
2,2-bis(benzyloxymethyl)-3-fluoro-1-(((2-nitrophenyl)selenyl)methyl)cyclopropane

Guidance literature:: With tributylphosphine; In tetrahydrofuran; at 20 ℃; for 4h;
DOI:10.1080/15257770701257210

Reference yield:

: 1012785-60-2
2,2-bis(benzyloxymethyl)-3-bromo-1-tert-butyldimethylsilyloxymethyl-3-fluorocyclopropane

: 1012785-62-4
2,2-bis(benzyloxymethyl)-3-fluoro-1-(((2-nitrophenyl)selenyl)methyl)cyclopropane

Guidance literature:: Multi-step reaction with 3 steps

1: 83 percent / AIBN; Bu₃SnH / 4 h / Heating

2: 94 percent / Bu₄NF / tetrahydrofuran / 8 h / 20 °C

3: 91 percent / Bu₃P / tetrahydrofuran / 4 h / 20 °C

With 2,2'-azobis(isobutyronitrile); tributylphosphine; tetrabutyl ammonium fluoride; tri-n-butyl-tin hydride; In tetrahydrofuran;
DOI:10.1080/15257770701257210

Reference yield:

: 1012785-61-3
(+/-)-tert-Butyldimethylsilyl-[2,2-bis(benzyloxymethyl)-3-fluorocyclopropyl]methanol

: 1012785-62-4
2,2-bis(benzyloxymethyl)-3-fluoro-1-(((2-nitrophenyl)selenyl)methyl)cyclopropane

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / Bu₄NF / tetrahydrofuran / 8 h / 20 °C

2: 91 percent / Bu₃P / tetrahydrofuran / 4 h / 20 °C

With tributylphosphine; tetrabutyl ammonium fluoride; In tetrahydrofuran;
DOI:10.1080/15257770701257210