C₁₃H₁₅PS₂

Base Information

Chemical Name:C₁₃H₁₅PS₂
CAS No.:1358777-92-0
Molecular Formula:C₁₃H₁₅PS₂
Molecular Weight:266.368
Hs Code.:

C<sub>13</sub>H<sub>15</sub>PS<sub>2</sub>

Synonyms:C₁₃H₁₅PS₂

Suppliers and Price of C₁₃H₁₅PS₂

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₁₃H₁₅PS₂

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₁₃H₁₅PS₂

There total 1 articles about C₁₃H₁₅PS₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 30540-36-4
3,4-dimethyl-1-phenylphosphole

: 74-88-4
methyl iodide

: 1358777-92-0
C₁₃H₁₅PS₂

Guidance literature:: 3,4-dimethyl-1-phenylphosphole; With potassium tert-butylate; In tetrahydrofuran; at 150 ℃; for 24h; Inert atmosphere; sealed pressure tube;

With sulfur; In tetrahydrofuran; at 20 ℃; for 0.25h; Inert atmosphere;

methyl iodide; at 20 ℃; Inert atmosphere;
DOI:10.1021/ol300113z

Reference yield: 52.0%

: 623-73-4
diazoacetic acid ethyl ester

: 1358777-92-0
C₁₃H₁₅PS₂

: 1358777-93-1
C₁₇H₂₁O₂PS₂

Guidance literature:: In 5,5-dimethyl-1,3-cyclohexadiene; at 145 ℃; for 1.25h; Inert atmosphere;
DOI:10.1021/ol300113z

Reference yield:

: 1358777-92-0
C₁₃H₁₅PS₂

: 1292834-38-8
C₁₆H₁₇O₂P

Guidance literature:: Multi-step reaction with 2 steps

1: 5,5-dimethyl-1,3-cyclohexadiene / 1.25 h / 145 °C / Inert atmosphere

2: triphenyl phosphite / 96 h / 160 °C / Inert atmosphere

With triphenyl phosphite; In 5,5-dimethyl-1,3-cyclohexadiene;
DOI:10.1021/ol300113z