Technology Process of C39H39O8P
There total 4 articles about C39H39O8P which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
dibenzyl erythronic acid benzyl ester; Dibenzyl N,N-diisopropylphosphoramidite;
With
1H-tetrazole;
In
acetonitrile;
at 4 ℃;
for 1h;
With
tert.-butylhydroperoxide;
In
decane; acetonitrile;
at 4 ℃;
for 2h;
DOI:10.1016/j.tetlet.2011.02.045
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: silver(l) oxide / diethyl ether / 12 h / 25 °C
2.1: lithium hydroxide monohydrate / water / 48 h / 4 °C
2.2: Dowex 50W-X12 / 0.33 h / 4 °C
3.1: dichloromethane
4.1: 1H-tetrazole / acetonitrile / 1 h / 4 °C
4.2: 2 h / 4 °C
With
1H-tetrazole; lithium hydroxide monohydrate; silver(l) oxide;
In
diethyl ether; dichloromethane; water; acetonitrile;
DOI:10.1016/j.tetlet.2011.02.045
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: 2,4,6-trimethylbenzenesulfonohydrazide / benzene / 2 h / Reflux
1.2: 0.67 h / Reflux
2.1: dichloromethane
3.1: 1H-tetrazole / acetonitrile / 1 h / 4 °C
3.2: 2 h / 4 °C
With
1H-tetrazole; 2,4,6-trimethylbenzenesulfonohydrazide;
In
dichloromethane; acetonitrile; benzene;
DOI:10.1016/j.tetlet.2011.02.045