2,2,2-trimethyl-1-trimethylsiloxy-1-phenyl-1-(2,4,6-tri-iso-propylphenyl)-disilane

Base Information

Chemical Name:2,2,2-trimethyl-1-trimethylsiloxy-1-phenyl-1-(2,4,6-tri-iso-propylphenyl)-disilane
CAS No.:934179-49-4
Molecular Formula:C₂₇H₄₆OSi₃
Molecular Weight:470.918
Hs Code.:

Synonyms:2,2,2-trimethyl-1-trimethylsiloxy-1-phenyl-1-(2,4,6-tri-iso-propylphenyl)-disilane

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Chemical Property of 2,2,2-trimethyl-1-trimethylsiloxy-1-phenyl-1-(2,4,6-tri-iso-propylphenyl)-disilane

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Technology Process of 2,2,2-trimethyl-1-trimethylsiloxy-1-phenyl-1-(2,4,6-tri-iso-propylphenyl)-disilane

There total 2 articles about 2,2,2-trimethyl-1-trimethylsiloxy-1-phenyl-1-(2,4,6-tri-iso-propylphenyl)-disilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 14.0%

: 934179-44-9
1-chloro-3,3,3-trimethyl-1-phenyl-1-(2,4,6-tri-iso-propylphenyl)disiloxane

: 75-77-4
chloro-trimethyl-silane

: 1,1,1,3,3,3-hexamethyl-2-phenyl-2-(2,4,6-tri-iso-propylphenyl)-trisilane

: 1,1,1,5,5,5-hexamethyl-3-phenyl-3-(2,4,6-tri-iso-propyl-phenyl)-trisiloxane

: 934179-49-4
2,2,2-trimethyl-1-trimethylsiloxy-1-phenyl-1-(2,4,6-tri-iso-propylphenyl)-disilane

Guidance literature:: 1-chloro-3,3,3-trimethyl-1-phenyl-1-(2,4,6-tri-iso-propylphenyl)disiloxane; With lithium; In tetrahydrofuran; at -78 ℃; for 2.5h;

chloro-trimethyl-silane; In tetrahydrofuran; at -78 - 20 ℃; for 24.5h;
DOI:10.1016/j.jorganchem.2006.11.033

Reference yield:

: 107742-36-9
Dichloro(phenyl)(2,4,6-triisopropylphenyl)silane

: 934179-49-4
2,2,2-trimethyl-1-trimethylsiloxy-1-phenyl-1-(2,4,6-tri-iso-propylphenyl)-disilane

Guidance literature:: Multi-step reaction with 2 steps

1.1: pentane; diethyl ether / -78 °C

2.1: lithium / tetrahydrofuran / 2.5 h / -78 °C

2.2: 47 percent / tetrahydrofuran / 24.5 h / -78 - 20 °C

With lithium; In tetrahydrofuran; diethyl ether; pentane;
DOI:10.1016/j.jorganchem.2006.11.033

Reference yield: 64.0%

: 934179-49-4
2,2,2-trimethyl-1-trimethylsiloxy-1-phenyl-1-(2,4,6-tri-iso-propylphenyl)-disilane

: 1066-35-9
dimethylmonochlorosilane

: 1,1,1,3,3-pentamethyl-2-phenyl-2-(2,4,6-tri-iso-propylphenyl)-trisilane

Guidance literature:: 2,2,2-trimethyl-1-trimethylsiloxy-1-phenyl-1-(2,4,6-tri-iso-propylphenyl)-disilane; With lithium; In tetrahydrofuran; at -78 ℃; for 44h;

dimethylmonochlorosilane; In tetrahydrofuran; at 20 ℃; for 24h;
DOI:10.1016/j.jorganchem.2006.11.033