(E)-1-bromo-2-phenyl-1-(trimethylsilyl)-1-butene

Base Information

Chemical Name:(E)-1-bromo-2-phenyl-1-(trimethylsilyl)-1-butene
CAS No.:96212-84-9
Molecular Formula:C₁₃H₁₉BrSi
Molecular Weight:283.283
Hs Code.:

Synonyms:(E)-1-bromo-2-phenyl-1-(trimethylsilyl)-1-butene

Suppliers and Price of (E)-1-bromo-2-phenyl-1-(trimethylsilyl)-1-butene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Matrix Scientific
(E)-(1-Bromo-2-phenylbut-1-en-1-yl)trimethylsilane 97%
10g
$ 2160.00

Crysdot
(E)-(1-Bromo-2-phenylbut-1-en-1-yl)trimethylsilane 95+%
5g
$ 1340.00

Crysdot
(E)-(1-Bromo-2-phenylbut-1-en-1-yl)trimethylsilane 95+%
10g
$ 2143.00

Chemenu
(E)-(1-Bromo-2-phenylbut-1-en-1-yl)trimethylsilane 95%
10g
$ 2020.00

Chemenu
(E)-(1-Bromo-2-phenylbut-1-en-1-yl)trimethylsilane 95%
5g
$ 1262.00

Total 3 raw suppliers

Chemical Property of (E)-1-bromo-2-phenyl-1-(trimethylsilyl)-1-butene

Chemical Property:

Purity/Quality:: (E)-(1-Bromo-2-phenylbut-1-en-1-yl)trimethylsilane 97% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (E)-1-bromo-2-phenyl-1-(trimethylsilyl)-1-butene

There total 2 articles about (E)-1-bromo-2-phenyl-1-(trimethylsilyl)-1-butene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 3536-96-7
vinylmagnesium chloride

: 2170-06-1
1-Phenyl-2-(trimethylsilyl)acetylene

: 96212-84-9
(E)-1-bromo-2-phenyl-1-(trimethylsilyl)-1-butene

Guidance literature:: vinylmagnesium chloride; In tetrahydrofuran; hexane; at 20 ℃; for 0.5h;

1-Phenyl-2-(trimethylsilyl)acetylene; In tetrahydrofuran; hexane; at 55 ℃; for 3h;

With bromine; In tetrahydrofuran; hexane; at 20 ℃; for 0.166667h; Further stages.;
DOI:10.1021/ja077992u

Reference yield:

: 96-10-6
diethylaluminium chloride

: 2170-06-1
1-Phenyl-2-(trimethylsilyl)acetylene

: 96212-84-9
(E)-1-bromo-2-phenyl-1-(trimethylsilyl)-1-butene

Guidance literature:: With bis(cyclopentadienyl)titanium dichloride; N-Bromosuccinimide; Yield given. Multistep reaction; 1.) CH₂Cl₂, RT, 6 h, 2.) from -70 deg C to -78 deg C, 0.5 h;
DOI:10.1021/jo00212a023