6-O-acetyl-2,3,4,5-tetra-O-benzyl-D-altrose propane-1,3-diyldithioacetal

Base Information

Chemical Name:6-O-acetyl-2,3,4,5-tetra-O-benzyl-D-altrose propane-1,3-diyldithioacetal
CAS No.:1427016-82-7
Molecular Formula:C₃₉H₄₄O₆S₂
Molecular Weight:672.907
Hs Code.:

Synonyms:6-O-acetyl-2,3,4,5-tetra-O-benzyl-D-altrose propane-1,3-diyldithioacetal

Suppliers and Price of 6-O-acetyl-2,3,4,5-tetra-O-benzyl-D-altrose propane-1,3-diyldithioacetal

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 6-O-acetyl-2,3,4,5-tetra-O-benzyl-D-altrose propane-1,3-diyldithioacetal

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 6-O-acetyl-2,3,4,5-tetra-O-benzyl-D-altrose propane-1,3-diyldithioacetal

There total 3 articles about 6-O-acetyl-2,3,4,5-tetra-O-benzyl-D-altrose propane-1,3-diyldithioacetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1427016-81-6
2,3,4,5-tetra-O-benzyl-D-altrose propane-1,3-diyl dithioacetal

: 75-36-5
acetyl chloride

: 1427016-82-7
6-O-acetyl-2,3,4,5-tetra-O-benzyl-D-altrose propane-1,3-diyldithioacetal

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃;
DOI:10.1021/jo400130p

Reference yield:

: 1427016-79-2
6-O-trityl-D-altrose propane-1,3-diyl dithioacetal

: 1427016-82-7
6-O-acetyl-2,3,4,5-tetra-O-benzyl-D-altrose propane-1,3-diyldithioacetal

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil; N,N-dimethyl-formamide / 0.5 h / 20 °C

1.2: 20 °C

2.1: sulfuric acid; methanol / dichloromethane / 20 °C

3.1: triethylamine / dichloromethane / 0 - 20 °C

With methanol; sulfuric acid; sodium hydride; triethylamine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; mineral oil;
DOI:10.1021/jo400130p

Reference yield:

: 1427016-80-5
2,3,4,5-tetra-O-benzyl-6-O-trityl-D-altrose propane-1,3-diyldithioacetal

: 1427016-82-7
6-O-acetyl-2,3,4,5-tetra-O-benzyl-D-altrose propane-1,3-diyldithioacetal

Guidance literature:: Multi-step reaction with 2 steps

1: sulfuric acid; methanol / dichloromethane / 20 °C

2: triethylamine / dichloromethane / 0 - 20 °C

With methanol; sulfuric acid; triethylamine; In dichloromethane;
DOI:10.1021/jo400130p