toluene-4-sulfonic acid (R)-2-(4-fluoro-3-trifluoromethyl-phenyl)-2-hydroxyethyl ester

Base Information

Chemical Name:toluene-4-sulfonic acid (R)-2-(4-fluoro-3-trifluoromethyl-phenyl)-2-hydroxyethyl ester
CAS No.:1598382-65-0
Molecular Formula:C₁₆H₁₄F₄O₄S
Molecular Weight:378.344
Hs Code.:

Synonyms:toluene-4-sulfonic acid (R)-2-(4-fluoro-3-trifluoromethyl-phenyl)-2-hydroxyethyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of toluene-4-sulfonic acid (R)-2-(4-fluoro-3-trifluoromethyl-phenyl)-2-hydroxyethyl ester

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Technology Process of toluene-4-sulfonic acid (R)-2-(4-fluoro-3-trifluoromethyl-phenyl)-2-hydroxyethyl ester

There total 2 articles about toluene-4-sulfonic acid (R)-2-(4-fluoro-3-trifluoromethyl-phenyl)-2-hydroxyethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1598382-64-9
toluene-4-sulfonic acid 2-(4-fluoro-3-trifluoromethyl-phenyl)-2-oxo-ethyl ester

: 1598382-65-0
toluene-4-sulfonic acid (R)-2-(4-fluoro-3-trifluoromethyl-phenyl)-2-hydroxyethyl ester

Guidance literature:: With borane-THF; (3aR)-1-methyl-3,3-diphenyl-tetrahydro-pyrrolo[1,2-c][1,3,2]oxazaborole; In tetrahydrofuran; at 20 ℃; for 1.5h;

Reference yield:

: 27126-76-7
[hydroxy(tosyloxy)iodo]benzene

: 208173-24-4
1-(4-fluoro-3-(trifluoromethyl)phenyl)ethanone

: 1598382-65-0
toluene-4-sulfonic acid (R)-2-(4-fluoro-3-trifluoromethyl-phenyl)-2-hydroxyethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: acetonitrile / 5 h / Reflux

2: borane-THF; (3aR)-1-methyl-3,3-diphenyl-tetrahydro-pyrrolo[1,2-c][1,3,2]oxazaborole / tetrahydrofuran / 1.5 h / 20 °C

With borane-THF; (3aR)-1-methyl-3,3-diphenyl-tetrahydro-pyrrolo[1,2-c][1,3,2]oxazaborole; In tetrahydrofuran; acetonitrile;