1-tert-butyldiphenylsilyloxy-1'-tert-butyldimethylsilyloxy-2,4'-methylenediphenol

Base Information

Chemical Name:1-tert-butyldiphenylsilyloxy-1'-tert-butyldimethylsilyloxy-2,4'-methylenediphenol
CAS No.:197805-67-7
Molecular Formula:C₃₅H₄₄O₂Si₂
Molecular Weight:552.904
Hs Code.:

Synonyms:1-tert-butyldiphenylsilyloxy-1'-tert-butyldimethylsilyloxy-2,4'-methylenediphenol

Suppliers and Price of 1-tert-butyldiphenylsilyloxy-1'-tert-butyldimethylsilyloxy-2,4'-methylenediphenol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-tert-butyldiphenylsilyloxy-1'-tert-butyldimethylsilyloxy-2,4'-methylenediphenol

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Technology Process of 1-tert-butyldiphenylsilyloxy-1'-tert-butyldimethylsilyloxy-2,4'-methylenediphenol

There total 3 articles about 1-tert-butyldiphenylsilyloxy-1'-tert-butyldimethylsilyloxy-2,4'-methylenediphenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 58479-61-1
tert-butylchlorodiphenylsilane

: 197805-63-3
2-[4-(tert-Butyl-dimethyl-silanyloxy)-benzyl]-phenol

: 197805-67-7
1-tert-butyldiphenylsilyloxy-1'-tert-butyldimethylsilyloxy-2,4'-methylenediphenol

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; for 24h;
DOI:10.1016/S0040-4020(97)00903-4

Reference yield:

: 2467-03-0
2-[(4-hydroxyphenyl)methyl]phenol

: 197805-67-7
1-tert-butyldiphenylsilyloxy-1'-tert-butyldimethylsilyloxy-2,4'-methylenediphenol

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / imidazole / dimethylformamide / 1 h / Ambient temperature

2: 98 percent / imidazole / dimethylformamide / 24 h

With 1H-imidazole; In N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(97)00903-4

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: 197805-67-7
1-tert-butyldiphenylsilyloxy-1'-tert-butyldimethylsilyloxy-2,4'-methylenediphenol

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / imidazole / dimethylformamide / 1 h / Ambient temperature

2: 98 percent / imidazole / dimethylformamide / 24 h

With 1H-imidazole; In N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(97)00903-4