-benzol

Base Information

• Chemical Name: -benzol
• CAS No.: 38634-91-2
• Molecular Formula: C₃₄H₂₇IO₄
• Molecular Weight: 626.49

Synonyms:-benzol

Chemical Property of -benzol

Chemical Property:

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Technology Process of -benzol

There total 2 articles about -benzol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

[bis(acetoxy)iodo]benzene (3240-34-4) + 2,2-diphenylacetic acid (117-34-0) → -benzol (38634-91-2)

Guidance literature:

In chlorobenzene; under 25 - 35 Torr;

Reference yield:

2,2-diphenylacetic acid (117-34-0) + iodosylbenzene (536-80-1) → -benzol (38634-91-2)

Guidance literature:

DOI:10.1021/ja00770a033

Reference yield: 25.0%

3,3-Dimethylbut-1-yne (917-92-0) + -benzol (38634-91-2) → 3,3-dimethylbutynyl diphenylacetate (113779-52-5)

Guidance literature:

With n-butyllithium; t-butylnitrite; In tetrahydrofuran; at -78 ℃; for 0.5h;

DOI:10.1021/ja00218a043

upstream raw materials:

[bis(acetoxy)iodo]benzene

2,2-diphenylacetic acid

iodosylbenzene

Downstream raw materials:

3,3-dimethylbutynyl diphenylacetate

1-propynyl diphenylacetate

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