(3S)-3-hydroxy-2,2-dimethylpent-4-enyl benzoate

Base Information

Chemical Name:(3S)-3-hydroxy-2,2-dimethylpent-4-enyl benzoate
CAS No.:725738-51-2
Molecular Formula:C₁₄H₁₈O₃
Molecular Weight:234.295
Hs Code.:

Synonyms:(3S)-3-hydroxy-2,2-dimethylpent-4-enyl benzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3S)-3-hydroxy-2,2-dimethylpent-4-enyl benzoate

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Technology Process of (3S)-3-hydroxy-2,2-dimethylpent-4-enyl benzoate

There total 1 articles about (3S)-3-hydroxy-2,2-dimethylpent-4-enyl benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (3R)-3-(tert-butyldimethylsilyloxy)-2,2-dimethyl-5-trimethylsilylpentane-1,4-diol

: 725738-51-2
(3S)-3-hydroxy-2,2-dimethylpent-4-enyl benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / BF₃*Et₂O / CH₂Cl₂ / 15 h / 20 °C

2: 73 percent / polymer-supported-1,5,7-triazabicyclo[4.4.0]dec-5-ene / CH₂Cl₂ / 5 h / 20 °C

With 7-methyl-1,5,7-triazabicyclo[4.4.0]dec-5-ene on polystyrene.HL; boron trifluoride diethyl etherate; In dichloromethane;
DOI:10.1002/chem.200305669

Reference yield:

: 725738-51-2
(3S)-3-hydroxy-2,2-dimethylpent-4-enyl benzoate

: 725738-52-3
(3S)-3,5-dihydroxy-2,2-dimethylpentyl benzoate

Guidance literature:: (3S)-3-hydroxy-2,2-dimethylpent-4-enyl benzoate; With borane-THF; In tetrahydrofuran; at 20 ℃; for 20h;

With polymer-supported triethylamine carbonate; polymer-supported trimethylamine thiosulfate; dihydrogen peroxide; In tetrahydrofuran; methanol;
DOI:10.1002/chem.200305669

Reference yield:

: 725738-51-2
(3S)-3-hydroxy-2,2-dimethylpent-4-enyl benzoate

: 725738-53-4
(3S)-3,5-bis-(tert-butyldimethylsilyloxy)-2,2-dimethylpentyl benzoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: BH₃*THF / tetrahydrofuran / 20 h / 20 °C

1.2: 850 mg / polymer-supported triethylamine carbonate; aq. H₂O₂; polymer-supported trimethylamine thiosulfate / tetrahydrofuran; methanol

2.1: 98 percent / morpholinomethyl polystyrene / CH₂Cl₂ / 20 h / 20 °C

With borane-THF; morpholinomethyl polystyrene; In tetrahydrofuran; dichloromethane;
DOI:10.1002/chem.200305669