Technology Process of (3S)-3,5-dihydroxy-2,2-dimethylpentyl benzoate
There total 4 articles about (3S)-3,5-dihydroxy-2,2-dimethylpentyl benzoate which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
(3S)-3-hydroxy-2,2-dimethylpent-4-enyl benzoate;
With
borane-THF;
In
tetrahydrofuran;
at 20 ℃;
for 20h;
With
polymer-supported triethylamine carbonate; polymer-supported trimethylamine thiosulfate; dihydrogen peroxide;
In
tetrahydrofuran; methanol;
DOI:10.1002/chem.200305669
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: 73 percent / polymer-supported-1,5,7-triazabicyclo[4.4.0]dec-5-ene / CH2Cl2 / 5 h / 20 °C
2.1: BH3*THF / tetrahydrofuran / 20 h / 20 °C
2.2: 850 mg / polymer-supported triethylamine carbonate; aq. H2O2; polymer-supported trimethylamine thiosulfate / tetrahydrofuran; methanol
With
borane-THF; 7-methyl-1,5,7-triazabicyclo[4.4.0]dec-5-ene on polystyrene.HL;
In
tetrahydrofuran; dichloromethane;
DOI:10.1002/chem.200305669
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: 73 percent / polymer-supported-1,5,7-triazabicyclo[4.4.0]dec-5-ene / CH2Cl2 / 5 h / 20 °C
2.1: BH3*THF / tetrahydrofuran / 20 h / 20 °C
2.2: 850 mg / polymer-supported triethylamine carbonate; aq. H2O2; polymer-supported trimethylamine thiosulfate / tetrahydrofuran; methanol
With
borane-THF; 7-methyl-1,5,7-triazabicyclo[4.4.0]dec-5-ene on polystyrene.HL;
In
tetrahydrofuran; dichloromethane;
DOI:10.1002/chem.200305669
