Carbonic acid (S)-2-((S)-2-benzyl-3-methyl-butyrylamino)-3-phenyl-propyl ester methyl ester

Base Information

Chemical Name:Carbonic acid (S)-2-((S)-2-benzyl-3-methyl-butyrylamino)-3-phenyl-propyl ester methyl ester
CAS No.:444722-10-5
Molecular Formula:C₂₃H₂₉NO₄
Molecular Weight:383.488
Hs Code.:

Synonyms:Carbonic acid (S)-2-((S)-2-benzyl-3-methyl-butyrylamino)-3-phenyl-propyl ester methyl ester

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Chemical Property of Carbonic acid (S)-2-((S)-2-benzyl-3-methyl-butyrylamino)-3-phenyl-propyl ester methyl ester

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Technology Process of Carbonic acid (S)-2-((S)-2-benzyl-3-methyl-butyrylamino)-3-phenyl-propyl ester methyl ester

There total 3 articles about Carbonic acid (S)-2-((S)-2-benzyl-3-methyl-butyrylamino)-3-phenyl-propyl ester methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 67-56-1
methanol

: 117037-09-9
(S)-4-Benzyl-3-((S)-2-benzyl-3-methyl-butyryl)-oxazolidin-2-one

: 444722-10-5
Carbonic acid (S)-2-((S)-2-benzyl-3-methyl-butyrylamino)-3-phenyl-propyl ester methyl ester

Guidance literature:: With sodium azide; at 20 ℃; for 24h;
DOI:10.1016/S0040-4039(02)00155-7

Reference yield:

: 145589-03-3,104266-90-2
(S)-4-benzyl-3-(3-methylbutanoyl)oxazolidin-2-one

: 444722-10-5
Carbonic acid (S)-2-((S)-2-benzyl-3-methyl-butyrylamino)-3-phenyl-propyl ester methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / NaHMDS / tetrahydrofuran / 4 h / -40 °C

2: 51 percent / sodium azide / 24 h / 20 °C

With sodium azide; sodium hexamethyldisilazane; In tetrahydrofuran;
DOI:10.1016/S0040-4039(02)00155-7

Reference yield:

: 100-39-0
benzyl bromide

: 444722-10-5
Carbonic acid (S)-2-((S)-2-benzyl-3-methyl-butyrylamino)-3-phenyl-propyl ester methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / NaHMDS / tetrahydrofuran / 4 h / -40 °C

2: 51 percent / sodium azide / 24 h / 20 °C

With sodium azide; sodium hexamethyldisilazane; In tetrahydrofuran;
DOI:10.1016/S0040-4039(02)00155-7