C₁₁H₅NO₄BrCl₃

Base Information

Chemical Name:C₁₁H₅NO₄BrCl₃
CAS No.:947612-45-5
Molecular Formula:C₁₁H₅BrCl₃NO₄
Molecular Weight:401.428
Hs Code.:

C<sub>11</sub>H<sub>5</sub>NO<sub>4</sub>BrCl<sub>3</sub>

Synonyms:C₁₁H₅NO₄BrCl₃

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Chemical Property of C₁₁H₅NO₄BrCl₃

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Technology Process of C₁₁H₅NO₄BrCl₃

There total 4 articles about C₁₁H₅NO₄BrCl₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 916978-57-9
6-bromo-2-nitrophenylacetylene

: 17341-93-4
2,2,2-Trichloroethyl chloroformate

: 947612-45-5
C₁₁H₅NO₄BrCl₃

Guidance literature:: 6-bromo-2-nitrophenylacetylene; With lithium diisopropyl amide; In tetrahydrofuran; hexane; at -78 ℃; for 0.166667h;

2,2,2-Trichloroethyl chloroformate; In tetrahydrofuran; hexane; at -78 - 20 ℃; Further stages.;
DOI:10.1021/ja071163r

Reference yield:

: 20357-21-5
2-bromo-6-nitrobenzaldehyde

: 947612-45-5
C₁₁H₅NO₄BrCl₃

Guidance literature:: Multi-step reaction with 2 steps

1.1: 85 percent / K₂CO₃; methanol / 2 h / 20 °C

2.1: LDA / tetrahydrofuran; hexane / 0.17 h / -78 °C

2.2: 68 percent / tetrahydrofuran; hexane / -78 - 20 °C

With methanol; potassium carbonate; lithium diisopropyl amide; In tetrahydrofuran; hexane;
DOI:10.1021/ja071163r

Reference yield:

2-bromo-6-nitrotoluene: 55289-35-5
2-bromo-6-nitrotoluene

: 947612-45-5
C₁₁H₅NO₄BrCl₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: dimethylformamide / 16 h / 135 °C

2.1: 3.44 g / NaIO₄ / dimethylformamide; H₂O / 22 h / 0 - 20 °C

3.1: 85 percent / K₂CO₃; methanol / 2 h / 20 °C

4.1: LDA / tetrahydrofuran; hexane / 0.17 h / -78 °C

4.2: 68 percent / tetrahydrofuran; hexane / -78 - 20 °C

With methanol; sodium periodate; potassium carbonate; lithium diisopropyl amide; In tetrahydrofuran; hexane; water; N,N-dimethyl-formamide;
DOI:10.1021/ja071163r