(+/-)-3-<(4-Tertio-butyl dimethylsiloxy)-3-methoxybenzyl>butan-4-olide

Base Information

Chemical Name:(+/-)-3-<(4-Tertio-butyl dimethylsiloxy)-3-methoxybenzyl>butan-4-olide
CAS No.:140193-23-3
Molecular Formula:C₁₈H₂₈O₄Si
Molecular Weight:336.503
Hs Code.:

Synonyms:(+/-)-3-<(4-Tertio-butyl dimethylsiloxy)-3-methoxybenzyl>butan-4-olide

Suppliers and Price of (+/-)-3-<(4-Tertio-butyl dimethylsiloxy)-3-methoxybenzyl>butan-4-olide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (+/-)-3-<(4-Tertio-butyl dimethylsiloxy)-3-methoxybenzyl>butan-4-olide

Chemical Property:

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Technology Process of (+/-)-3-<(4-Tertio-butyl dimethylsiloxy)-3-methoxybenzyl>butan-4-olide

There total 2 articles about (+/-)-3-<(4-Tertio-butyl dimethylsiloxy)-3-methoxybenzyl>butan-4-olide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 84755-40-8
(hydroxy-4 methoxy-3 benzyl)-4 dihydro-3H-furannone-2

: 18162-48-6
tert-butyldimethylsilyl chloride

: 140193-23-3
(+/-)-3-<(4-Tertio-butyl dimethylsiloxy)-3-methoxybenzyl>butan-4-olide

Guidance literature:: With dmap; triethylamine; In dichloromethane; for 16h; Ambient temperature;
DOI:10.1016/S0040-4020(01)88129-1

Reference yield:

: 92831-74-8
4-<<4-(benzyloxy)-3-methoxyphenyl>methyl>dihydro-2(3H)-furanone

: 140193-23-3
(+/-)-3-<(4-Tertio-butyl dimethylsiloxy)-3-methoxybenzyl>butan-4-olide

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / Pd/C

2: imidazole / dimethylformamide / 20 °C

With 1H-imidazole; hydrogen; palladium on activated charcoal; In N,N-dimethyl-formamide;
DOI:10.1039/b304411d