C₁₃H₁₇NO₃

Base Information

• Chemical Name: C₁₃H₁₇NO₃
• CAS No.: 1606993-67-2
• Molecular Formula: C₁₃H₁₇NO₃
• Molecular Weight: 235.283
• Mol file: 1606993-67-2.mol

Synonyms:C₁₃H₁₇NO₃

Chemical Property of C₁₃H₁₇NO₃

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of C₁₃H₁₇NO₃

There total 1 articles about C₁₃H₁₇NO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

4-methoxy-aniline (104-94-9) + ethyl 2,4-dibromobutyrate (36847-51-5) → C13H17NO3 (1606993-67-2)

Guidance literature:

With N,N,N,N,N,N-hexamethylphosphoric triamide; sodium hydrogencarbonate; In water; N,N-dimethyl-formamide; at 100 ℃; for 4h;

DOI:10.1021/jo500249c

Reference yield: 73.0%

C13H17NO3 (1606993-67-2) + methyl iodide (74-88-4) → N-(4-methoxyphenyl)-2-ethoxycarbonyl-2-methylazetidine (1606993-73-0)

Guidance literature:

C₁₃H₁₇NO₃; With lithium diisopropyl amide; In tetrahydrofuran; hexane; at -78 ℃; for 0.25h; Inert atmosphere;

methyl iodide; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 0.5h; Inert atmosphere;

DOI:10.1021/jo500249c

Reference yield:

C13H17NO3 (1606993-67-2) → N-(4-methoxyphenyl)-2-formylazetidine (1606993-66-1)

Guidance literature:

With diisobutylaluminium hydride; In tetrahydrofuran; toluene; at -78 ℃; for 2h; Inert atmosphere;

DOI:10.1021/jo500249c

upstream raw materials:

4-methoxy-aniline

ethyl 2,4-dibromobutyrate

Downstream raw materials:

N-(4-methoxyphenyl)-2-vinylazetidine

C₁₉H₁₉NO₂

C₁₃H₁₇NO

N-(4-methoxyphenyl)-2-formylazetidine