1,2-bis((4-((1H-pyrazol-1-yl)methyl)-1H-1,2,3-triazol-1-yl)methyl)benzene

Base Information

Chemical Name:1,2-bis((4-((1H-pyrazol-1-yl)methyl)-1H-1,2,3-triazol-1-yl)methyl)benzene
CAS No.:1609103-15-2
Molecular Formula:C₂₀H₂₀N₁₀
Molecular Weight:400.446
Hs Code.:

Synonyms:1,2-bis((4-((1H-pyrazol-1-yl)methyl)-1H-1,2,3-triazol-1-yl)methyl)benzene

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Chemical Property of 1,2-bis((4-((1H-pyrazol-1-yl)methyl)-1H-1,2,3-triazol-1-yl)methyl)benzene

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Technology Process of 1,2-bis((4-((1H-pyrazol-1-yl)methyl)-1H-1,2,3-triazol-1-yl)methyl)benzene

There total 3 articles about 1,2-bis((4-((1H-pyrazol-1-yl)methyl)-1H-1,2,3-triazol-1-yl)methyl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 20306-74-5
1-(prop-2-yn-1-yl)-1H-pyrazole

: 102437-79-6
1,2-bis(azidomethyl)benzene

: 1609103-15-2
1,2-bis((4-((1H-pyrazol-1-yl)methyl)-1H-1,2,3-triazol-1-yl)methyl)benzene

Guidance literature:: With copper(ll) sulfate pentahydrate; sodium L-ascorbate; In dimethyl sulfoxide; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1039/c3dt53295j

Reference yield:

: 623-24-5
1,4-bis(bromomethyl)benzene

: 1609103-15-2
1,2-bis((4-((1H-pyrazol-1-yl)methyl)-1H-1,2,3-triazol-1-yl)methyl)benzene

Guidance literature:: Multi-step reaction with 2 steps

1: sodium azide / dimethyl sulfoxide / 24 h / 20 °C / Inert atmosphere; Schlenk technique

2: copper(ll) sulfate pentahydrate; sodium L-ascorbate / dimethyl sulfoxide / 2 h / 20 °C / Inert atmosphere

With sodium azide; copper(ll) sulfate pentahydrate; sodium L-ascorbate; In dimethyl sulfoxide;
DOI:10.1039/c3dt53295j

Reference yield:

: 91-13-4
α,α'-dibromo-o-xylene

: 1609103-15-2
1,2-bis((4-((1H-pyrazol-1-yl)methyl)-1H-1,2,3-triazol-1-yl)methyl)benzene

Guidance literature:: Multi-step reaction with 2 steps

1: sodium azide / dimethyl sulfoxide / 3 h / 20 °C / Inert atmosphere; Schlenk technique

2: copper(ll) sulfate pentahydrate; sodium L-ascorbate / dimethyl sulfoxide / 2 h / 20 °C / Inert atmosphere

With sodium azide; copper(ll) sulfate pentahydrate; sodium L-ascorbate; In dimethyl sulfoxide;
DOI:10.1039/c3dt53295j