C₄₄H₆₈O₈Si

Base Information

• Chemical Name: C₄₄H₆₈O₈Si
• CAS No.: 1000788-24-8
• Molecular Formula: C₄₄H₆₈O₈Si
• Molecular Weight: 753.105
• Mol file: 1000788-24-8.mol

Synonyms:C₄₄H₆₈O₈Si

Chemical Property of C₄₄H₆₈O₈Si

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of C₄₄H₆₈O₈Si

There total 1 articles about C₄₄H₆₈O₈Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

methanol (67-56-1) + C41H62O6Si (918410-16-9) + ethyl acetate (141-78-6) → C44H68O8Si (1000788-24-8)

Guidance literature:

C₄₁H₆₂O₆Si; ethyl acetate; With lithium diisopropyl amide; In tetrahydrofuran; hexane; at -78 - -42 ℃;

methanol; With citric acid; at 70 ℃; for 2h;

With lithium hydroxide; In tetrahydrofuran; methanol; water; Further stages.;

DOI:10.1021/jo701821h

Reference yield:

C44H68O8Si (1000788-24-8) → C43H62O6Si + C44H66O7Si (918410-25-0)

Guidance literature:

C₄₄H₆₈O₈Si; With 2,4,6-trichlorobenzoyl chloride; triethylamine; In tetrahydrofuran; at 20 ℃; for 15h;

With dmap; In toluene; at 110 ℃; for 0.5h; Further stages. Title compound not separated from byproducts.;

DOI:10.1021/jo701821h

Reference yield:

methanol (67-56-1) + C44H68O8Si (1000788-24-8) → C43H62O6Si + C44H66O7Si (918410-25-0)

Guidance literature:

C₄₄H₆₈O₈Si; With 2,4,6-trichlorobenzoyl chloride; triethylamine; In tetrahydrofuran; at 20 ℃; for 15h;

With dmap; In toluene; at 110 ℃; for 0.5h;

methanol; With citric acid; at 70 ℃; for 72h; Further stages. Title compound not separated from byproducts.;

DOI:10.1021/jo701821h

upstream raw materials:

methanol

C₄₁H₆₂O₆Si

ethyl acetate

Downstream raw materials:

C₄₄H₆₆O₇Si