1,2-O-isopropylidene-3-O-(2-naphthylmethyl)-6-deoxy-6-C-vinyl-α-D-galactofuranose

Base Information

Chemical Name:1,2-O-isopropylidene-3-O-(2-naphthylmethyl)-6-deoxy-6-C-vinyl-α-D-galactofuranose
CAS No.:1352234-66-2
Molecular Formula:C₂₂H₂₆O₅
Molecular Weight:370.445
Hs Code.:

Synonyms:1,2-O-isopropylidene-3-O-(2-naphthylmethyl)-6-deoxy-6-C-vinyl-α-D-galactofuranose

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Chemical Property of 1,2-O-isopropylidene-3-O-(2-naphthylmethyl)-6-deoxy-6-C-vinyl-α-D-galactofuranose

Chemical Property:

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Technology Process of 1,2-O-isopropylidene-3-O-(2-naphthylmethyl)-6-deoxy-6-C-vinyl-α-D-galactofuranose

There total 2 articles about 1,2-O-isopropylidene-3-O-(2-naphthylmethyl)-6-deoxy-6-C-vinyl-α-D-galactofuranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1352234-51-5
1,2-O-isopropylidene-3-O-(2-naphthylmethyl)-β-L-arabinopentodialdofuranose

: 24850-33-7
allyltributylstanane

: 1352234-57-1
(3aR,4aS,5S,7R,8aS,8bR)-5-(benzyloxy)-2,2-dimethylhexahydro[1,3]dioxolo[4,5-b]benzofuran-7,8a(4aH)-diol

: 1352234-66-2
1,2-O-isopropylidene-3-O-(2-naphthylmethyl)-6-deoxy-6-C-vinyl-α-D-galactofuranose

: 1352234-52-6
1,2-O-isopropylidene-3-O-(2-naphthylmethyl)-6-deoxy-6-C-vinyl-β-L-altrofuranose

Guidance literature:: 1,2-O-isopropylidene-3-O-(2-naphthylmethyl)-β-L-arabinopentodialdofuranose; With magnesium bromide diethyl etherate; In dichloromethane; at -78 ℃; for 0.0833333h;

allyltributylstanane; In dichloromethane; at 78 ℃; for 3h; Concentration; Overall yield = 74 %; diastereoselective reaction;
DOI:10.1021/jo401166q

Reference yield:

: 1352234-51-5
1,2-O-isopropylidene-3-O-(2-naphthylmethyl)-β-L-arabinopentodialdofuranose

: 762-72-1
allyl-trimethyl-silane

: 1352234-57-1
(3aR,4aS,5S,7R,8aS,8bR)-5-(benzyloxy)-2,2-dimethylhexahydro[1,3]dioxolo[4,5-b]benzofuran-7,8a(4aH)-diol

: 1352234-66-2
1,2-O-isopropylidene-3-O-(2-naphthylmethyl)-6-deoxy-6-C-vinyl-α-D-galactofuranose

: 1352234-52-6
1,2-O-isopropylidene-3-O-(2-naphthylmethyl)-6-deoxy-6-C-vinyl-β-L-altrofuranose

Guidance literature:: 1,2-O-isopropylidene-3-O-(2-naphthylmethyl)-β-L-arabinopentodialdofuranose; With magnesium bromide diethyl etherate; In dichloromethane; at -78 ℃; for 0.0833333h;

allyl-trimethyl-silane; In dichloromethane; at 78 ℃; for 3h; Overall yield = 86 %; diastereoselective reaction;
DOI:10.1021/jo401166q

Reference yield: 91.0%

: 1352234-66-2
1,2-O-isopropylidene-3-O-(2-naphthylmethyl)-6-deoxy-6-C-vinyl-α-D-galactofuranose

: 100-39-0
benzyl bromide

: 1352234-67-3
C₂₉H₃₂O₅

Guidance literature:: With tetra-(n-butyl)ammonium iodide; sodium hydride; In tetrahydrofuran; N,N-dimethyl-formamide; mineral oil; at 0 - 20 ℃; for 4h;
DOI:10.1021/jo401166q