2,7-Dichloro-6-(2-hydroxy-ethyl)-4-(2-nitro-phenyl)-quinoline-5,8-dione

Base Information

Chemical Name:2,7-Dichloro-6-(2-hydroxy-ethyl)-4-(2-nitro-phenyl)-quinoline-5,8-dione
CAS No.:156489-04-2
Molecular Formula:C₁₇H₁₀Cl₂N₂O₅
Molecular Weight:393.183
Hs Code.:

Synonyms:2,7-Dichloro-6-(2-hydroxy-ethyl)-4-(2-nitro-phenyl)-quinoline-5,8-dione

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Chemical Property of 2,7-Dichloro-6-(2-hydroxy-ethyl)-4-(2-nitro-phenyl)-quinoline-5,8-dione

Chemical Property:

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Technology Process of 2,7-Dichloro-6-(2-hydroxy-ethyl)-4-(2-nitro-phenyl)-quinoline-5,8-dione

There total 10 articles about 2,7-Dichloro-6-(2-hydroxy-ethyl)-4-(2-nitro-phenyl)-quinoline-5,8-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 156489-03-1
4,7-Dichloro-9-(2-nitro-phenyl)-2,3-dihydro-furo[2,3-f]quinolin-5-ol

: 156489-04-2
2,7-Dichloro-6-(2-hydroxy-ethyl)-4-(2-nitro-phenyl)-quinoline-5,8-dione

Guidance literature:: With nitric acid; In acetic acid;
DOI:10.1021/jo00092a002

Reference yield:

: 13391-30-5
2,3-dihydro-5-methoxybenzofuran

: 156489-04-2
2,7-Dichloro-6-(2-hydroxy-ethyl)-4-(2-nitro-phenyl)-quinoline-5,8-dione

Guidance literature:: Multi-step reaction with 8 steps

1: 81 percent / HNO₃ / acetic acid

2: 100 percent / H₂ / Pd-C

3: 83 percent / m-xylene / Heating

4: 82 percent / 80percent H₂SO₄ / 75 °C

5: 94 percent / POCl₃ / 50 °C

6: 83 percent / HNO₃ / acetic acid

7: 80 percent / POCl₃ / CHCl₃

8: 79 percent / HNO₃ / acetic acid

With sulfuric acid; hydrogen; nitric acid; trichlorophosphate; palladium on activated charcoal; In chloroform; acetic acid; m-xylene;
DOI:10.1021/jo00092a002

Reference yield:

: 156488-97-0
2,3-Dihydro-5-methoxy-6-nitrobenzofuran

: 156489-04-2
2,7-Dichloro-6-(2-hydroxy-ethyl)-4-(2-nitro-phenyl)-quinoline-5,8-dione

Guidance literature:: Multi-step reaction with 7 steps

1: 100 percent / H₂ / Pd-C

2: 83 percent / m-xylene / Heating

3: 82 percent / 80percent H₂SO₄ / 75 °C

4: 94 percent / POCl₃ / 50 °C

5: 83 percent / HNO₃ / acetic acid

6: 80 percent / POCl₃ / CHCl₃

7: 79 percent / HNO₃ / acetic acid

With sulfuric acid; hydrogen; nitric acid; trichlorophosphate; palladium on activated charcoal; In chloroform; acetic acid; m-xylene;
DOI:10.1021/jo00092a002