Acetic acid 2-[2,7-dichloro-4-(2-nitro-phenyl)-5,8-dioxo-5,8-dihydro-quinolin-6-yl]-ethyl ester

Base Information

Chemical Name:Acetic acid 2-[2,7-dichloro-4-(2-nitro-phenyl)-5,8-dioxo-5,8-dihydro-quinolin-6-yl]-ethyl ester
CAS No.:156489-06-4
Molecular Formula:C₁₉H₁₂Cl₂N₂O₆
Molecular Weight:435.22
Hs Code.:

Synonyms:Acetic acid 2-[2,7-dichloro-4-(2-nitro-phenyl)-5,8-dioxo-5,8-dihydro-quinolin-6-yl]-ethyl ester

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Chemical Property of Acetic acid 2-[2,7-dichloro-4-(2-nitro-phenyl)-5,8-dioxo-5,8-dihydro-quinolin-6-yl]-ethyl ester

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Technology Process of Acetic acid 2-[2,7-dichloro-4-(2-nitro-phenyl)-5,8-dioxo-5,8-dihydro-quinolin-6-yl]-ethyl ester

There total 11 articles about Acetic acid 2-[2,7-dichloro-4-(2-nitro-phenyl)-5,8-dioxo-5,8-dihydro-quinolin-6-yl]-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 75-36-5
acetyl chloride

: 156489-04-2
2,7-Dichloro-6-(2-hydroxy-ethyl)-4-(2-nitro-phenyl)-quinoline-5,8-dione

: 156489-06-4
Acetic acid 2-[2,7-dichloro-4-(2-nitro-phenyl)-5,8-dioxo-5,8-dihydro-quinolin-6-yl]-ethyl ester

Guidance literature:: With pyridine; In dichloromethane;
DOI:10.1021/jo00092a002

Reference yield:

: 13391-30-5
2,3-dihydro-5-methoxybenzofuran

: 156489-06-4
Acetic acid 2-[2,7-dichloro-4-(2-nitro-phenyl)-5,8-dioxo-5,8-dihydro-quinolin-6-yl]-ethyl ester

Guidance literature:: Multi-step reaction with 9 steps

1: 81 percent / HNO₃ / acetic acid

2: 100 percent / H₂ / Pd-C

3: 83 percent / m-xylene / Heating

4: 82 percent / 80percent H₂SO₄ / 75 °C

5: 94 percent / POCl₃ / 50 °C

6: 83 percent / HNO₃ / acetic acid

7: 80 percent / POCl₃ / CHCl₃

8: 79 percent / HNO₃ / acetic acid

9: 96 percent / pyridine / CH₂Cl₂

With pyridine; sulfuric acid; hydrogen; nitric acid; trichlorophosphate; palladium on activated charcoal; In dichloromethane; chloroform; acetic acid; m-xylene;
DOI:10.1021/jo00092a002

Reference yield:

: 156488-97-0
2,3-Dihydro-5-methoxy-6-nitrobenzofuran

: 156489-06-4
Acetic acid 2-[2,7-dichloro-4-(2-nitro-phenyl)-5,8-dioxo-5,8-dihydro-quinolin-6-yl]-ethyl ester

Guidance literature:: Multi-step reaction with 8 steps

1: 100 percent / H₂ / Pd-C

2: 83 percent / m-xylene / Heating

3: 82 percent / 80percent H₂SO₄ / 75 °C

4: 94 percent / POCl₃ / 50 °C

5: 83 percent / HNO₃ / acetic acid

6: 80 percent / POCl₃ / CHCl₃

7: 79 percent / HNO₃ / acetic acid

8: 96 percent / pyridine / CH₂Cl₂

With pyridine; sulfuric acid; hydrogen; nitric acid; trichlorophosphate; palladium on activated charcoal; In dichloromethane; chloroform; acetic acid; m-xylene;
DOI:10.1021/jo00092a002